piperidine in methanol T=50°C; Knoevenagel condensation; 8 h; Inert atmosphere;

titanium tetrachloride; zinc in tetrahydrofuran T=20°C;

hydrogen in N,N-dimethyl-formamide T=20°C; P=1500.15 Torr; 24 h; Autoclave;

1: Pd nanoparticle core coated by amine funtionalized metal organic framesworks / N,N-dimethyl-formamide / 0.33 h / 20 °C / |Autoclave 2: hydrogen / N,N-dimethyl-formamide / 24 h / 20 °C / 1500.15 Torr / |Autoclave View Scheme

lead(IV) acetate; acetic acid; N,N-dimethyl-formamide

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