1-苯基-乙酮 2-(2,4-二硝基苯基)腙合成路线 （共 27 条）
反应条件
1: sec-phenethyl alcohol With peracetic acid; C9H17NO5S(1-)*C11H12IN2(1+); acetic acid in hexafluoroisopropyl alcohol T=20°C; 10 h; 2: (2,4-dinitro-phenyl)-hydrazine With sulfuric acid in diethyl ether; ethanol; water
参考文献
Tetrahedron Letters, , vol. 53, # 12 p. 1438 - 1444
反应条件
acetic acid in ethanol 1 h; Heating;
参考文献
Monatshefte fur Chemie, , vol. 127, # 11 p. 1115 - 1122
反应条件
1: R(1+)*BF4(1-); air / acetonitrile / 16 h / UV-irradiation 2: HCl / acetonitrile; diethyl ether; H2O View Scheme
参考文献
Journal of Organic Chemistry, , vol. 70, # 24 p. 9780 - 9788
反应条件
toluene-4-sulfonic acid in ethanol Heating;
参考文献
Chemische Berichte, , vol. 113, # 6 p. 2081 - 2085
反应条件
1: pyridine; 2,2,6,6-tetramethyl-1-piperidinyloxy, free radical / water; acetonitrile / 3 h / 50 °C 2: sulfuric acid / ethanol; water; acetonitrile View Scheme
参考文献
Tetrahedron Letters, , vol. 52, # 16 p. 1952 - 1955
反应条件
1: 1-amino-1-phenylethane With cycloundeca[b]pyrimido[5,4-d]pyrrole12,14-dione derivative in acetonitrile 16 h; Irradiation; 2: (2,4-dinitro-phenyl)-hydrazine With hydrogenchloride
参考文献
Journal of Organic Chemistry, , vol. 69, # 4 p. 1256 - 1261
反应条件
hydrogenchloride in diethyl ether
参考文献
Journal of Organic Chemistry, , vol. 69, # 26 p. 9184 - 9190
反应条件
1: 1,1,4-triphenylpenta-1,3-diene With potassium permanganate in acetone 0.5 h; Reflux; 2: (2,4-dinitro-phenyl)-hydrazine
参考文献
Helvetica Chimica Acta, , vol. 91, # 5 p. 783 - 804
反应条件
hydrogen; boric acid; acetone; W-2 Raney-Ni 1.) methanol, water, 25 deg C, 8h; Yield given. Multistep reaction;
参考文献
Journal of Organic Chemistry, , vol. 49, p. 1654 - 1656
反应条件
1: 89 percent / butyl-lithium / tetrahydrofuran; hexane / 0 - 20 °C 2: 93 percent / m-chloroperbenzoic acid / CH2Cl2 / -23 °C 3: 84 percent / butyl-lithium / hexane; tetrahydrofuran / 0 °C 4: 85 percent / lithium aluminum hydride / tetrahydrofuran / 2 h / Heating 5: 85percent m-chloroperbenzoic acid / CH2Cl2 / 1.5 h / -23 °C View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 195 - 204
