(±)-2-氯-1-苯基乙醇合成路线 （共 94 条）
反应条件
sulfuric acid; sodium chloride; sodium periodate in water; acetonitrile T=70°C; 18 h;
参考文献
Council of Scientific and Industrial Research
Patent: US6825383 B1, 2004 ;
Location in patent: Page column 7 ;
反应条件
1: chloromethyl iodide With isopropylmagnesium chloride lithium chloride complex in tetrahydrofuran T=-78°C; 0.166667 h; Inert atmosphere; 2: benzaldehyde in tetrahydrofuran T=-78°C; 0.5 h; Inert atmosphere; ConcentrationTime;
参考文献
Nishimura, Rodolfo H.V.; Toledo, Fabiano T.; Lopes, Joao L.C.; Clososki, Giuliano C.
Tetrahedron Letters, 2013 , vol. 54, # 4 p. 287 - 290
反应条件
sec-phenethyl alcohol; 4 A molecular sieve; trimethylaluminum; 2,7-dimethyl-1,8-biphenylenediol in hexane; dichloromethane 2.) r.t., 2 h;
参考文献
Ooi, Takashi; Miura, Tomoya; Itagaki, Yoshifumi; Ichikawa, Hayato; Maruoka, Keiji
Synthesis, 2002 , # 2 p. 279 - 291
反应条件
hydrogenchloride; β-cyclodextrin in methanol; water; acetone T=20°C; 12 h;
参考文献
Reddy, M.Arjun; Surendra; Bhanumathi; Rao, K.Rama
Tetrahedron, 2002 , vol. 58, # 30 p. 6003 - 6008
反应条件
methyllithium in tetrahydrofuran; diethyl ether T=-78°C; 1 h;
参考文献
Kapeller, Dagmar C.; Hammerschmidt, Friedrich
Journal of the American Chemical Society, 2008 , vol. 130, # 7 p. 2329 - 2335
反应条件
2,4,6-trichloro-1,3,5-triazine; N,N-dimethyl-formamide in dichloromethane T=25°C; 0.25 h;
参考文献
De Luca, Lidia; Giacomelli, Giampaolo; Porcheddu, Andrea
Organic Letters, 2002 , vol. 4, # 4 p. 553 - 555
反应条件
sodium periodate; sulfuric acid; lithium bromide in water; acetonitrile T=25°C; pH=6.12;
参考文献
Dewkar, Gajanan K.; Narina, Srinivasarao V.; Sudalai, Arumugam
Organic Letters, 2003 , vol. 5, # 23 p. 4501 - 4504
反应条件
lithium in tetrahydrofuran T=-50°C; 0.333333 h; Irradiation;
参考文献
Einhorn, Cathy; Allavena, Corinne; Luche, Jean-Louis
Journal of the Chemical Society, Chemical Communications, 1988 , # 5 p. 333 - 334
反应条件
[Ir(η5-C5Me5)(C6H4-2-CH2NHCH3)(NCCH3)](PF6); potassium tert-butylate in water; toluene T=20°C; 1 h; Inert atmosphere;
参考文献
Journal of the American Chemical Society, , vol. 130, # 41 p. 13508 - 13509
反应条件
lithium dimesityl borohydride bis(dimethoxyethane) in ethylene glycol dimethyl ether T=23°C; 2 h; Title compound not separated from byproducts;
参考文献
Journal of Organic Chemistry, , vol. 58, # 25 p. 7138 - 7142
