1,2-双(二苯基膦)乙烷合成路线 (共 132 条)
反应条件
in tetrahydrofuran T=50°C; 2 h; Thermodynamic data;
参考文献
Canadian Journal of Chemistry, , vol. 79, # 5-6 p. 626 - 631
反应条件
palladium diacetate in nitrogen
参考文献
Mitsubishi Kasei Corporation
Patent: US5159082 A1, 1992 ;
反应条件
in methanol; isopropyl alcohol in warm soln.; washing with ether, drying in vac.;
参考文献
Gmelin Handbook: Ni: MVol.C2, 8.20, page 1073 - 1085
反应条件
in ethanol in warm soln.; diamagnetic form obtained from the filtrate of the paramagnetic form;
参考文献
Booth, G.; Chatt, J.
Journal of the Chemical Society, 1965 , p. 3238 - 3241
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Gmelin Handbook: Ni: MVol.C2, 8.20, page 1073 - 1085
反应条件
in chloroform dppe was added to Pt complexin CHCl3 and left to stand at 0°C for20 min;
参考文献
Bokach, Nadezhda A.; Kukushkin, Vadim Yu.; Haukka, Matti; Frausto da Silva, Joao J. R.; Pombeiro, Armando J. L.
Inorganic Chemistry, 2003 , vol. 42, # 11 p. 3602 - 3608
反应条件
in dichloromethane byproducts: quinoline N-oxide, 1,3,5,7-cyclooctatetraene; addn. of org. compd. to soln. of Rh compd., room temp.; evapn. (vac.), addn. Et2O, filtration, washing (Et2O);
参考文献
Stiakaki, Maria-Aglaia; Christofides, Aristides
Gazzetta Chimica Italiana, 1990 , vol. 120, p. 809 - 812
反应条件
2: ethanol View Scheme
参考文献
Gmelin Handbook: Rh: SVol.B3, 4.26.2.4, page 175 - 179
反应条件
in acetone Irradiation (UV/VIS); under Ar or N2, irradn. of soln.; 1H NMR spectroscopy;
参考文献
Inorganic Chemistry, , vol. 26, p. 253 - 258
反应条件
in tetrahydrofuran T=20°C; 5 h;
参考文献
Phosphorus, Sulfur and Silicon and the Related Elements, , vol. 188, # 6 p. 726 - 738
反应条件
in toluene room temp.;
参考文献
Gambarotta, Sandro; Chiesi-Villa, Angiola; Guastini, Carlo
Inorganic Chemistry, 1988 , vol. 27, p. 99 - 102