1,2-双(二苯基膦)乙烷合成路线 （共 132 条）
反应条件
sodium; palladium diacetate in nitrogen
参考文献
Mitsubishi Kasei Corporation
Patent: US5159082 A1, 1992 ;
反应条件
sodium polisulfide in methanol; acetone 0.0833333 h; Ambient temperature;
参考文献
Miranda; Salas; Mondragon; Velasco
Synthetic Communications, 1992 , vol. 22, # 7 p. 1077 - 1080
反应条件
sulfur in tetrahydrofuran 18 h;
参考文献
Faller; Fontaine, Philip P.
Journal of Organometallic Chemistry, 2007 , vol. 692, # 5 p. 976 - 982
反应条件
in tetrahydrofuran T=20°C;
参考文献
Boulos, Leila S.; Ewies, Ewies F.; Fahmy, Amin F. M.
Phosphorus, Sulfur and Silicon and the Related Elements, 2013 , vol. 188, # 6 p. 726 - 738
反应条件
in tetrahydrofuran mixt. was heated under reflux for 3 h; mixt. was filtered hot, ppt. was washed with THF and THF/hexane, dried in vac., filtrate was kept for 3 days at room temp., filtered, ppt. was washed and dried; elem. anal.;
参考文献
Evans, David J.; Hitchcock, Peter B.; Leigh; Nicholson, Brian K.; Niedwieski, Antonio C.; Nunes, Fabio S.; Soares, Jaisa F.
Inorganica Chimica Acta, 2001 , vol. 319, # 1-2 p. 147 - 158
反应条件
in chloroform; acetone ligand soln. in CHCl3 and FeCl2 in acetone refluxed for 20 h; ppt. septd., MAS;
参考文献
Long, Ella M.; Brown, Neil J.; Man, Wing Y.; Fox, Mark A.; Yufit, Dmitry S.; Howard, Judith A.K.; Low, Paul J.
Inorganica Chimica Acta, 2012 , vol. 380, # 1 p. 358 - 371
反应条件
1: diethyl ether 2: dichloromethane 3: dichloromethane View Scheme
参考文献
Hawrelak, Eric J.; Bernskoetter, Wesley H.; Lobkovsky, Emil; Yee, Gordon T.; Bill, Eckhard; Chirik, Paul J.
Inorganic Chemistry, 2005 , vol. 44, # 9 p. 3103 - 3111
反应条件
in toluene 7 h; Reflux;
参考文献
Boulos, Leila S.; Ewies, Ewies F.; Fahmy, Amin F. M.
Phosphorus, Sulfur and Silicon and the Related Elements, 2013 , vol. 188, # 6 p. 726 - 738
反应条件
in acetone addn. of soln. of dppe (1 equiv.) in acetone to suspn. of (AuCl(SMe)2) (2 equiv.) in acetone; stirring for 2 h; pptn., filtration, washing with acetone, diethyl ether and pentane, drying under vac.;
参考文献
Brandys, Marie-Claude; Jennings, Michael C.; Puddephatt, Richard J.
Journal of the Chemical Society, Dalton Transactions, 2000 , # 24 p. 4601 - 4606
反应条件
in not given N2-atmosphere; stoich. amts.;
参考文献
Molter, Anja; Rust, Joerg; Lehmann, Christian W.; Deepa, Ganesh; Chiba, Peter; Mohr, Fabian
Dalton Transactions, 2011 , vol. 40, # 38 p. 9810 - 9820
