1,2-双(二苯基膦)乙烷合成路线 (共 132 条)
反应条件
1: 68 percent / Li / tetrahydrofuran / 0.75 h / 760 Torr / Heating
2: tetrahydrofuran / 0.75 h / Heating
View Scheme
参考文献
Bautista, Maria Teresa; Earl, Kelly Anne; Maltby, Patricia Anne; Morris, Robert Harold; Schweitzer, Caroline Theresia
Canadian Journal of Chemistry, 1994 , vol. 72, # 3 p. 547 - 560
反应条件
in acetonitrile
under N2, reflux in Soxhlet apparatus; ppt., elem. anal.;
参考文献
Clark, Deborah A.; Jones, David L.; Mawby, Roger J.
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1980 , p. 565 - 569
参考文献
Clark, Deborah A.; Jones, David L.; Mawby, Roger J.
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1980 , p. 565 - 569
反应条件
dihydrogen peroxide in dichloromethane; water
0.0833333 h;
参考文献
Petersson, Maria J.; Loughlin, Wendy A.; Jenkins, Ian D.
Chemical Communications, 2008 , # 37 p. 4493 - 4494
反应条件
in tetrahydrofuran
T=20°C; 5 h;
参考文献
Boulos, Leila S.; Ewies, Ewies F.; Fahmy, Amin F. M.
Phosphorus, Sulfur and Silicon and the Related Elements, 2013 , vol. 188, # 6 p. 726 - 738
反应条件
in tetrahydrofuran
T=20°C;
参考文献
Boulos, Leila S.; Ewies, Ewies F.; Fahmy, Amin F. M.
Phosphorus, Sulfur and Silicon and the Related Elements, 2013 , vol. 188, # 6 p. 726 - 738
反应条件
in tetrahydrofuran
T=20°C; 3 h;
参考文献
Boulos, Leila S.; Ewies, Ewies F.; Fahmy, Amin F. M.
Phosphorus, Sulfur and Silicon and the Related Elements, 2013 , vol. 188, # 6 p. 726 - 738
反应条件
in toluene
7 h; Reflux;
参考文献
Boulos, Leila S.; Ewies, Ewies F.; Fahmy, Amin F. M.
Phosphorus, Sulfur and Silicon and the Related Elements, 2013 , vol. 188, # 6 p. 726 - 738
反应条件
in toluene
7 h; Reflux;
参考文献
Boulos, Leila S.; Ewies, Ewies F.; Fahmy, Amin F. M.
Phosphorus, Sulfur and Silicon and the Related Elements, 2013 , vol. 188, # 6 p. 726 - 738
反应条件
in toluene
8 h; Reflux;
参考文献
Boulos, Leila S.; Ewies, Ewies F.; Fahmy, Amin F. M.
Phosphorus, Sulfur and Silicon and the Related Elements, 2013 , vol. 188, # 6 p. 726 - 738