1-甲氧基-4-苯氧基苯合成路线 （共 73 条）
反应条件
1: Cu / 195 °C
2: Fe, AcOH / H2O; methanol
3: (i) aq. HBr, NaNO2, (ii) CuBr, aq. HBr
4: Cu, 4-methoxy-phenol <K salt> / 220 - 230 °C
View Scheme
参考文献
Forrest,J.
Journal of the Chemical Society, 1960 , p. 581 - 588
反应条件
copper diacetate; copper
T=200 - 215°C;
参考文献
Walker
Journal of the Chemical Society, 1942 , p. 347,352
参考文献
Abramovitch, Rudolph A.; Alvernhe, Gerard; Bartnik, Romuald; Dassanayake, Nissanke L.; Inbasekaran, Mutiah N.; Kato, Shiego
Journal of the American Chemical Society, 1981 , vol. 103, # 15 p. 4558 - 4565
反应条件
in acetonitrile-D3
T=45°C; Inert atmosphereDarkness; regioselective reaction;
参考文献
Wang, Bijia; Graskemper, Joseph W.; Qin, Linlin; DiMagno, Stephen G.
Angewandte Chemie - International Edition, 2010 , vol. 49, # 24 p. 4079 - 4083
反应条件
in acetonitrile-D3
T=80°C; 12 h; Inert atmosphereDarkness; regioselective reaction;
参考文献
Wang, Bijia; Graskemper, Joseph W.; Qin, Linlin; DiMagno, Stephen G.
Angewandte Chemie - International Edition, 2010 , vol. 49, # 24 p. 4079 - 4083
反应条件
in acetonitrile-D3
T=45°C; Inert atmosphereDarkness; regioselective reaction;
参考文献
Wang, Bijia; Graskemper, Joseph W.; Qin, Linlin; DiMagno, Stephen G.
Angewandte Chemie - International Edition, 2010 , vol. 49, # 24 p. 4079 - 4083
参考文献
Hodgson; Foster
Journal of the Chemical Society, 1942 , p. 581
反应条件
1: (i) aq. HBr, NaNO2, (ii) CuBr, aq. HBr
2: Cu, 4-methoxy-phenol <K salt> / 220 - 230 °C
View Scheme
参考文献
Forrest,J.
Journal of the Chemical Society, 1960 , p. 581 - 588
反应条件
1: 2C2F3O2*2C11H12F3NO2Sn*O; potassium carbonate / 6 h / 200 °C
2: 2C2F3O2*2C11H12F3NO2Sn*O; potassium carbonate / 6 h / 200 °C
View Scheme
参考文献
Weidlich, Tomas; Dusek, Libor; Vystrcilova, Barbora; Eisner, Ales; Svec, Petr; Ruzicka, Ales
Applied Organometallic Chemistry, 2012 , vol. 26, # 6 p. 293 - 300
反应条件
2C2F3O2*2C11H12F3NO2Sn*O; potassium carbonate
T=200°C; 6 h;
参考文献
Weidlich, Tomas; Dusek, Libor; Vystrcilova, Barbora; Eisner, Ales; Svec, Petr; Ruzicka, Ales
Applied Organometallic Chemistry, 2012 , vol. 26, # 6 p. 293 - 300
