4,6-二氨基间苯二酚二盐酸盐合成路线 （共 11 条）
反应条件
hydrogenchloride; palladium in water
参考文献
The Dow Chemical Company
Patent: US5414130 A1, 1995 ;
反应条件
hydrogenchloride; palladium 10 on activated carbon; hydrogen in water T=20°C;
参考文献
Mike, Jared F.; Makowski, Andrew J.; Jeffries-El, Malika
Organic Letters, 2008 , vol. 10, # 21 p. 4915 - 4918
反应条件
hydrogen in hydrogenchloride; ethanol; water
参考文献
The Dow Chemical Company
Patent: US5453542 A1, 1995 ;
反应条件
hydrogenchloride; H2; sodium acetate; palladium over carbon in water; acetic acid
反应条件
ammonium acetate; hydrogenchloride; palladium monocarbide in water
反应条件
nitric acid in water; acetic acid
反应条件
palladium monocarbide in hydrogenchloride
反应条件
1: 1.) H2, conc. HCl, 2.) stannous chloride dihydrate, conc. HCl / 1.) 10percent Pd/C / 1.) H2O, 55 deg C, 4 h, 2.) 25 deg C 2: 94 percent / conc. HCl / 18 h / 150 °C View Scheme
参考文献
Journal of Organic Chemistry, , vol. 62, # 23 p. 8255 - 8256
反应条件
1: 1.) cumene hydroperoxide, NaOH, 2.) sodium hypophosphite / 1.) CH2Cl2, liquid NH3, -33 deg C, 1 h, 2.) -10 deg C; room temperature, 4 h 2: 1.) H2, conc. HCl, 2.) stannous chloride dihydrate, conc. HCl / 1.) 10percent Pd/C / 1.) H2O, 55 deg C, 4 h, 2.) 25 deg C 3: 94 percent / conc. HCl / 18 h / 150 °C View Scheme
参考文献
Journal of Organic Chemistry, , vol. 62, # 23 p. 8255 - 8256
参考文献
Evstaf'ev,V.P. et al.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1970 , vol. 6, p. 682 - 687
Khimiya Geterotsiklicheskikh Soedinenii, 1970 , vol. 6, # 6 p. 739 - 743
