反应条件
in benzene under N2 a soln. of Co-complex in benzene was trated with SnCl4 at roomtemp., stood for 2 d; filtered, pumped off, extd. with pentane, filtered, crystd. at -20°C from toluene/pentane; the pentane soln. was evapd. afforded Ph3GeCl;
参考文献
Journal of Organometallic Chemistry, , vol. 205, # 1 p. 31 - 45
