(E)-2,2,7,7-四甲基-2,7-二硅杂辛-4-烯合成路线 (共 19 条)
反应条件
maleic anhydride; palladium diacetate in dichloromethane T=30°C; Substitution; 17 h;
参考文献
Macsari, Istvan; Hupe, Eike; Szabo, Kalman J.
Journal of Organic Chemistry, 1999 , vol. 64, # 26 p. 9547 - 9556
反应条件
lithium in tetrahydrofuran T=0 - 10°C; 24 h;
参考文献
Meagher, Timothy P.; Shechter, Harold
Journal of Organic Chemistry, 1998 , vol. 63, # 13 p. 4193 - 4198
反应条件
bis(dibenzylideneacetone)-palladium(0) in tetrahydrofuran T=20°C; silylation; 12 h;
参考文献
Tsuji, Yasushi; Funato, Masahiro; Ozawa, Masakatsu; Ogiyama, Hiroaki; Kajita, Satoshi; Kawamura, Takashi
Journal of Organic Chemistry, 1996 , vol. 61, # 17 p. 5779 - 5787
反应条件
C70H88MoN2O2Si in benzene-d6 T=23°C; 0.33 h; Inert atmosphere;
参考文献
Jiang, Annie J.; Zhao, Yu; Schrock, Richard R.; Hoveyda, Amir H.
Journal of the American Chemical Society, 2009 , vol. 131, # 46 p. 16630 - 16631
反应条件
in toluene T=0°C; 4 h;
参考文献
Richter, Wolf Juergen; Neugebauer, Brigitte
Synthesis, 1985 , # 11 p. 1059 - 1060
反应条件
bis(cyclopentadienyl)titanium dichloride in tetrahydrofuran T=0°C; 0.166667 h;
参考文献
Watabe, Hiroyasu; Terao, Jun; Kambe, Nobuaki
Organic Letters, 2001 , vol. 3, # 11 p. 1733 - 1735
反应条件
bis(1,5-cyclooctadiene)nickel (0); diethylaluminium chloride; cyclohexa-1,3-diene; triphenylphosphine in toluene T=50°C; 48 h; Yield given. Yields of byproduct given;
参考文献
Cros, Philippe; Triantaphylides, Christian; Buono, Gerard
Journal of Organic Chemistry, 1988 , vol. 53, # 1 p. 185 - 187
反应条件
4,4'-di-tert-butylbiphenyl; lithium in tetrahydrofuran T=0°C; 0.75 h; Yield given. Yields of byproduct given;
参考文献
Guijarro, Albert; Yus, Miguel
Tetrahedron, 1994 , vol. 50, # 26 p. 7857 - 7864
反应条件
4,4'-di-tert-butylbiphenyl; lithium in tetrahydrofuran T=0°C; 0.75 h; Yield given. Yields of byproduct given;
参考文献
Guijarro, Albert; Yus, Miguel
Tetrahedron, 1994 , vol. 50, # 26 p. 7857 - 7864
反应条件
4,4'-di-tert-butylbiphenyl; lithium in tetrahydrofuran T=0°C; 0.75 h; Yield given. Yields of byproduct given;
参考文献
Guijarro, Albert; Yus, Miguel
Tetrahedron, 1994 , vol. 50, # 26 p. 7857 - 7864