全氟(2-甲基-2-戊烯) 合成路线 (共 126 条)
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反应条件
30320-27-5 1,1,1,4,4,5,5,5-八氟-3-(1,1,1,2,3,3,3-七氟丙烷-2-基)-2-(三氟甲基)戊-2-烯 +
反应条件
bis(.eta.(6)-benzene)chromium in benzene 24 h; other solvent; Product distributionMechanism;
参考文献
Journal of Organometallic Chemistry, , vol. 205, # 2 p. 185 - 191
反应条件
in various solvent(s) reactions of var. anions with var. reagents; Product distribution;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 201 - 208
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反应条件
30320-27-5 1,1,1,4,4,5,5,5-八氟-3-(1,1,1,2,3,3,3-七氟丙烷-2-基)-2-(三氟甲基)戊-2-烯 +
反应条件
π-bis(biphenyl)chromium(0) var. catalysts; Product distribution;
参考文献
Journal of Organometallic Chemistry, , vol. 218, # 2 p. 169 - 175
反应条件
triethylamine in acetonitrile 24 h; Heating;
参考文献
Yanagida, Shozo; Noji, Yukihiro; Okahara, Mitsuo
Bulletin of the Chemical Society of Japan, 1981 , vol. 54, # 4 p. 1151 - 1158
反应条件
water; triethylamine in acetonitrile T=45 - 60°C; 5 h;
参考文献
Cheburkov, Yuri; Moore, George G.I.
Journal of Fluorine Chemistry, 2003 , vol. 123, # 2 p. 227 - 231
反应条件
tris(2-methoxyethyl)amine; water in N,N-dimethyl-formamide
参考文献
Sud'enkov,Yu.Ya.
Journal of Organic Chemistry USSR (English Translation), 1978 , vol. 14, p. 1240 - 1241
Zhurnal Organicheskoi Khimii, 1978 , vol. 14, # 6 p. 1336 - 1337
反应条件
1: With triethylamine; tert-butyl alcohol T=55 - 60°C; 20 h; 2: With toluene-4-sulfonic acid T=110 - 115°C; 3 h; 3: With water; triethylamine Heating; Title compound not separated from byproducts;
参考文献
Cheburkov, Yuri; Moore, George G.I.
Journal of Fluorine Chemistry, 2003 , vol. 123, # 2 p. 227 - 231
反应条件
triethylamine T=40°C;
参考文献
Moldavskii; Bispen; Furin; Zhuzhgov
Russian Journal of Applied Chemistry, 1996 , vol. 69, # 4 p. 575 - 582
反应条件
NiF2; fluorine T=100°C;
参考文献
Zakharov, V. Yu.; Denisov, A. K.; Novikova, M. D.
Russian Journal of Organic Chemistry, 1994 , vol. 30, # 12 p. 1942 - 1945
Zhurnal Organicheskoi Khimii, 1994 , vol. 30, # 12 p. 1844 - 1846
反应条件
fluorine T=60 - 90°C; Fluorination; 0.666667 h; Product distribution; Further Variations:CatalystsTemperaturesSolvents;
参考文献
Moldavskii, Dmitrii D.; Bispen, Tatjana A.; Kaurova, Galina I.; Furin, Georgii G.
Journal of Fluorine Chemistry, 1999 , vol. 94, # 2 p. 157 - 167