双（1-金刚烷基）氯化磷合成路线 （共 12 条）
反应条件
tetrachloromethane T=50°C; 16 h;
参考文献
Koellhofer, Axel; Plenio, Herbert
Chemistry - A European Journal, 2003 , vol. 9, # 6 p. 1416 - 1425
反应条件
magnesium; phosphorus trichoride
参考文献
Beller, Matthias; Ehrentraut, Andreas; Ehrentraut, Wilhelm Hubert; Ehrentraut, Theresia Elisabeth; Fuhrmann, Christa; Zapf, Alexander
Patent: US2004/68131 A1, 2004 ;
反应条件
in diethyl ether Heating;
参考文献
Lavrova, E. A.; Koidan, G. N.; Marchenko, A. P.; Pinchuk, A. M.
Russian Journal of General Chemistry, 1994 , vol. 64, # 9.2 p. 1393 - 1394
Zhurnal Obshchei Khimii, 1994 , vol. 64, # 9 p. 1556 - 1557
反应条件
1: 94.3 percent / LiAlH4 / tetrahydrofuran / 16 h / Ambient temperature 2: 93.7 percent / COCl2, DBU / toluene / 16 h / Ambient temperature View Scheme
参考文献
Phosphorus, Sulfur and Silicon and the Related Elements, , vol. 102, # 1-4 p. 211 - 216
反应条件
1: 1.) PCl3, AlCl3, 2.) H2O / 1.) reflux, 6 h, 2.) chloroform 2: 94.3 percent / LiAlH4 / tetrahydrofuran / 16 h / Ambient temperature 3: 93.7 percent / COCl2, DBU / toluene / 16 h / Ambient temperature View Scheme
参考文献
Phosphorus, Sulfur and Silicon and the Related Elements, , vol. 102, # 1-4 p. 211 - 216
反应条件
phosphorus trichoride 24 h; Ambient temperature;
参考文献
Goerlich, Jens R.; Fischer, Axel; Jones, Peter G.; Schmutzler, Reinhard
Zeitschrift fuer Naturforschung, B: Chemical Sciences, 1994 , vol. 49, # 6 p. 801 - 811
反应条件
n-butyllithium in tetrahydrofuran; hexane
反应条件
in tetrahydrofuran; hexane Alkylation; 1 h; Heating;
参考文献
Synlett, , # 11 p. 1589 - 1592
反应条件
water; 1,8-diazabicyclo[5.4.0]undec-7-ene in dichloromethane 72 h; Ambient temperature;
参考文献
Goerlich, Jens R.; Schmutzler, Reinhard
Phosphorus, Sulfur and Silicon and the Related Elements, 1995 , vol. 102, # 1-4 p. 211 - 216
