反应条件
in neat (no solvent) condensation of 80 ml liquid SO2 on a mixt. of 200 g (NPCl2)3 and 300 g KF; heating at 98-100 °C for 22 days;; removal of an excess of SO2; fractionation, transition temp. 49-49.8 °C at 747 Torr; yield 115.3 (NPCl2)3;;
参考文献
Chapman, A. C.; Paddock, N. L.; Paine, D. H.; Searle, H. T.; Smith, D. R.
Journal of the Chemical Society, 1960 , p. 3608 - 3614
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Gmelin Handbook: P: MVol.C, 238, page 544 - 546
