(氯甲基)甲基-二氯硅烷合成路线 (共 42 条)
反应条件
chlorine Irradiation;
参考文献
Auner, N.; Grobe, J.
Journal of Organometallic Chemistry, 1980 , vol. 188, # 2 p. 151 - 178
反应条件
chlorine 15 h; HeatingIrradiation;
参考文献
Zeitschrift fuer Naturforschung, Teil B: Anorganische Chemie, Organische Chemie, , vol. 41, # 12 p. 1527 - 1534
反应条件
chlorine in not given Irradiation (UV/VIS); (CH3)2SiCl2 and Cl2 at 20-40°C under irradiation of light;;
参考文献
Journal of the American Chemical Society, , vol. 67, p. 1810 - 1812
反应条件
copper in diethyl ether (CH3)SiCl3 and diazomethane in ether above -30°C with Cu powder as catalyst;;
参考文献
Jukobovic, A. J.; Makarov, S. P.; etal.
Doklady Akad. Nauk SSSR. (russ.) (2), 1950 , vol. 71, p. 303 - 303
C. I, 1951 , p. 2419
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Gmelin Handbook: Si: MVol.C, 48, page 138 - 141
反应条件
YCl3; sulfuryl dichloride T=70°C; 10 h; Irradiationother catalysts (HoCl3,TmCl3); Product distribution;
参考文献
J. Gen. Chem. USSR (Engl. Transl.), , vol. 51, # 5 p. 1207 - 1208,1021
反应条件
T=24 - 40°C; UV-Licht.Irradiation;
参考文献
US2474578 , ;
Journal of the American Chemical Society, , vol. 67, p. 1810,1812
反应条件
tetrachloromethane; meta-chloroperoxybenzoic acid; chlorine 1) 80 deg C, 18 h; 2) 5-10 deg C; Multistep reaction;
参考文献
J. Gen. Chem. USSR (Engl. Transl.), , vol. 59, # 5.1 p. 1057 - 1062,934 - 937
反应条件
3-chloroprop-1-ene in tetrahydrofuran 3 h; Heating;
参考文献
J. Gen. Chem. USSR (Engl. Transl.), , vol. 58, # 7 p. 1599 - 1606,1425 - 1431
反应条件
H2O in ethanol; water boiling of (CH3)3SiOSi(CH3)3 and (CH3)(CH2Cl)SiCl2 (1:1 mol) in aq. alc. for 3 h;; washing of the soln. with H2O; drying over CaCl2; distn.;;
参考文献
Speier
Journal of the American Chemical Society, 1949 , vol. 71, p. 273
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Gmelin Handbook: Si: MVol.C, 104, page 286 - 288
参考文献
Speier
Journal of the American Chemical Society, 1949 , vol. 71, p. 273