N,N,N',N'-四苯基联苯胺合成路线 （共 19 条）
反应条件
potassium tert-butylate; [2,6-iPr2C6H3N=C(H)C(H)=NC6H3-2,6-iPr2]; copper(l) iodide in toluene T=120°C; 20 h;
参考文献
Tetrahedron Letters, , vol. 47, # 52 p. 9275 - 9278
反应条件
bis(1,5-cyclooctadiene)nickel (0); C{N(2,6-iPr2C6H3)CH}2 in tetrahydrofuran; 1,4-dioxane T=150°C; Kumada Cross-Coupling; 43 h; Inert atmosphere;
参考文献
Tetrahedron Letters, , vol. 53, # 41 p. 5531 - 5534
反应条件
tri-tert-butyl phosphine; caesium carbonate; cesium fluoride; tris-(dibenzylideneacetone)dipalladium(0); carbon dioxide in hexane T=100°C; P=93086.6 Torr; 48 h;
参考文献
Organic and Biomolecular Chemistry, , vol. 3, # 20 p. 3767 - 3781
反应条件
ethyl orthosilicate; caesium carbonate; copper(l) iodide T=145°C; Ullmann coupling reaction; 24 h;
参考文献
Chemical Communications, , # 30 p. 3186 - 3188
反应条件
palladium diacetate; potassium carbonate in ethanol; water T=20°C; Suzuki Coupling; 0.166667 h;
参考文献
RSC Advances, , vol. 3, # 2 p. 526 - 531
反应条件
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; palladium 10 on activated carbon; sodium t-butanolate in 1,3,5-trimethyl-benzene 24 h; Inert atmosphereReflux;
参考文献
Advanced Synthesis and Catalysis, , vol. 350, # 17 p. 2767 - 2777
反应条件
potassium hydroxide; copper in Soltrol/70reg; T=165°C; 7 h; Product distribution / selectivity;
参考文献
US2005/80292 A1, ;
Page/Page column 2 ;
反应条件
1: With Cu(II) perchlorate in acetonitrile T=25°C; 12 h; 2: With potassium carbonate in water; acetonitrile T=25°C; 0.5 h; Further stages.;
参考文献
Journal of Organic Chemistry, , vol. 73, # 8 p. 3245 - 3251
反应条件
1.1: n-BuLi / tetrahydrofuran; hexane / 0 °C 1.2: 91 percent / tetrahydrofuran; hexane / 18 h / 20 °C 2.1: 58 percent / P(t-Bu)3; Cs2CO3; CsF / Pd2dba3; scCO2 / hexane / 48 h / 100 °C / 93086.6 Torr View Scheme
参考文献
Organic and Biomolecular Chemistry, , vol. 3, # 20 p. 3767 - 3781
反应条件
toluene-4-sulfonic acid in toluene 12 h; Heating;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 59, # 3 p. 803 - 808
