(4-甲基苯氧基)乙酰氯合成路线 (共 13 条)
反应条件
thionyl chloride in benzene T=50°C; 3 h;
参考文献
Ito, Kazuaki; Takasawa, Toshiro; Ohba, Yoshihiro
Synthetic Communications, 2002 , vol. 32, # 24 p. 3839 - 3849
反应条件
in dichloromethane; N,N-dimethyl-formamide
参考文献
Sankyo Company, Limited
Patent: EP1354602 A1, 2003 ;
反应条件
1: alkali 2: thionyl chloride View Scheme
参考文献
Purohit; Srivastava
Journal of the Indian Chemical Society, 1991 , vol. 68, # 3 p. 163 - 165
反应条件
1: 70 percent / tetramethylammonium hydroxide / tetrahydrofuran; H2O / 24 h / Heating 2: 98 percent / thionyl chloride / benzene / 3 h / 50 °C View Scheme
参考文献
Ozcan, Sevil; Kazi, Aslamuzzaman; Marsilio, Frank; Fang, Bin; Guida, Wayne C.; Koomen, John; Lawrence, Harshani R.; Sebti, Said M.
Journal of Medicinal Chemistry, 2013 , vol. 56, # 10 p. 3783 - 3805
反应条件
1: ethyl acetate 2: thionyl chloride / 8 h / Heating View Scheme
参考文献
Jain; Srivastava
Journal of the Indian Chemical Society, 1990 , vol. 67, # 9 p. 775 - 776
参考文献
Chaurasia, Sunita; Srivastava, Savitri D.
Journal of the Indian Chemical Society, 1992 , vol. 69, # 1 p. 45 - 46
反应条件
2: phosphorus pentoxide View Scheme
参考文献
Higginbotham; Stephen
Journal of the Chemical Society, 1920 , vol. 117, p. 1541
参考文献
Higginbotham; Stephen
Journal of the Chemical Society, 1920 , vol. 117, p. 1541
反应条件
magnesium diethoxide
1.) Toluene, 3 h, reflux 2.) THF, reflux, 1 h; Yield given. Multistep reaction;
参考文献
Deshayes, Christian; Chabannet, Michel; Gelin, Suzanne
Journal of Heterocyclic Chemistry, 1986 , vol. 23, p. 1595 - 1598
参考文献
Shukla; Ahmad
Pharmazie, 1981 , vol. 36, # 5 p. 327 - 328