N-苯基苯羰基亚肼酰氯合成路线 (共 129 条)
参考文献
Fusco
Gazzetta Chimica Italiana, 1939 , vol. 69, p. 344,349
反应条件
triethylamine; 2-benzylidene-1-phenylhydrazine in benzene
T=20 - 25°C; 144 h; Further byproducts given;
参考文献
Buzykin, B. I.; Gazetdinova, N. G.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1980 , vol. 29, # 7 p. 1159 - 1163
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1980 , # 7 p. 1616 - 1620
反应条件
triethylamine in benzene
T=20 - 25°C; 144 h; Further byproducts given;
参考文献
Buzykin, B. I.; Gazetdinova, N. G.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1980 , vol. 29, # 7 p. 1159 - 1163
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1980 , # 7 p. 1616 - 1620
反应条件
in acetonitrile
15 h; Heating;
参考文献
Buzykin; Gubaidullin; Litvinov; Gazetdinova; Sysoeva
Russian Journal of General Chemistry, 1998 , vol. 68, # 12 p. 1889 - 1893
反应条件
1: Et3N / tetrahydrofuran
2: 19 percent / tetrahydrofuran / 8 h / Heating
View Scheme
参考文献
Bojilova, A.; Rodios, N. A.; Tsoleridis, C. A.; Alexandrou, N. E.
Journal of Heterocyclic Chemistry, 1990 , vol. 27, # 3 p. 735 - 738
反应条件
triethylamine in benzene
72 h; Heating; Title compound not separated from byproducts;
参考文献
Ballabio, Marzia; Croce, Piero Dalla; Massari, Valeria; Pocar, Donato; Riva, Alberto; Trimarco, Pasqualina
Journal of Chemical Research, Miniprint, 1983 , # 6 p. 1317 - 1340
反应条件
triethylamine in benzene
1 h; Heating; Further byproducts given;
参考文献
Moderhack, Dietrich; Lorke, Michael; Ernst, Ludger; Schomburg, Dietmar
Chemische Berichte, 1994 , vol. 127, # 9 p. 1633 - 1640
反应条件
1: 50 percent / Et3N / benzene / Ambient temperature
2: H2 / 5percent Pd/C / aq. ethanol / 760 Torr / Ambient temperature
3: NH2OH*HCl/AcONa / ethanol / 3 h / Heating
4: 92 percent / PCl5 / diethyl ether / 48 h / Ambient temperature
View Scheme
参考文献
Bianchi, Giorgio; Gandolfi, Remo; Micheli, Carlo De
Journal of Chemical Research, Miniprint, 1981 , # 1 p. 135 - 158
反应条件
triethylamine in benzene
40 h; Ambient temperature;
参考文献
Tsatsaroni, E, G.; Argyropoulos, N. G.; Alexandrou, N. E.; Houndas, A.; Terzis, A.
Journal of Heterocyclic Chemistry, 1984 , vol. 21, p. 701 - 704