反应条件
sulfuric acid; ammonium chloride in sulfuric acid byproducts: CH4; stirring of Me4Ge in concd. H2SO4 (0°C, 2 h, room temp., 5 h), cooling (ice bath), addn. of NH4Cl (over 30 min), stirring (1 h); extn. (pentane), drying (over Na2SO4), distn.;
参考文献
Barrau, J.; Rima, G.; El Amine, M.; Satge, J.
Synthesis and Reactivity in Inorganic and Metal-Organic Chemistry, 1988 , vol. 18, p. 21 - 28
