3-苯基-2-丙炔-1-醇合成路线 （共 165 条）
反应条件
pyridine in neat (no solvent) T=20°C; Sonogashira Cross-Coupling; 3 h;
参考文献
Bakherad, Mohammad; Keivanloo, Ali; Samangooei, Shahrzad
Tetrahedron Letters, 2012 , vol. 53, # 43 p. 5773 - 5776
反应条件
Cy3PAgCl; N-ethyl-N,N-diisopropylamine in water T=60°C; 12 h;
参考文献
Organic Letters, , vol. 7, # 20 p. 4395 - 4398
反应条件
1: phenylacetylene With 2,2,6,6-tetramethyl-piperidine; n-butyllithium in tetrahydrofuran T=-78°C; 1 h; 2: 1-Hydroxymethyl-1H-benzotriazole in tetrahydrofuran T=-78°C; 2 h;
参考文献
Deguest, Geoffrey; Bischoff, Laurent; Fruit, Corinne; Marsais, Francis
Organic Letters, 2007 , vol. 9, # 6 p. 1165 - 1167
反应条件
P(MeNCH2CH2)3N in methanol 0.333333 h; Ambient temperature;
参考文献
Ilankumaran, Palanichamy; Verkade
Journal of Organic Chemistry, 1999 , vol. 64, # 9 p. 3086 - 3089
反应条件
diisobutylaluminium hydride; triphenylphosphine; bis(acetylacetonate)nickel(II) in tetrahydrofuran T=20°C; Cycloaddition;
参考文献
Tetrahedron Letters, , vol. 40, # 28 p. 5231 - 5234
反应条件
1: phenylacetylene With n-butyllithium in tetrahydrofuran; hexanes T=-78°C; 0.833333 h; Inert atmosphere; 2: 2,4,6-trimethyl-1,3,5-trioxane T=-78 - 23°C; Inert atmosphere;
参考文献
Worthy, Amanda D.; Joe, Candice L.; Lightburn, Thomas E.; Tan, Kian L.
Journal of the American Chemical Society, 2010 , vol. 132, # 42 p. 14757 - 14759
反应条件
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; silver fluoride; sodium hydrogencarbonate in acetonitrile T=20°C; 3 h;
参考文献
Ye, Zhishi; Liu, Miaochang; Lin, Baoda; Wu, Huayue; Ding, Jinchang; Cheng, Jiang
Tetrahedron Letters, 2009 , vol. 50, # 5 p. 530 - 532
反应条件
lithium aluminium tetrahydride; diethyl ether
参考文献
Journal of the Chemical Society, , p. 1854,1858
反应条件
potassium tert-butylate in N,N-dimethyl-formamide 2 h; Ambient temperature;
参考文献
Yoshida, Masaaki; Hide, Tetsuro; Ohshima, Masabumi; Sasaki, Haruko; Toda, Takashi
Heterocycles, 1992 , vol. 33, # 2 p. 507 - 510
反应条件
AgNO2 in acetonitrile T=0 - 5°C; 54 h;
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 16, p. 1148 - 1150
Zhurnal Organicheskoi Khimii, , vol. 16, # 6 p. 1328 - 1330
