[二氟(苯基)甲基](三甲基)硅烷合成路线 （共 8 条）
反应条件
Cu-Mg in 10,11-dihydro-5-[3-(methylamino)propyl]-5H-dibenz(b,f)azepin T=25°C; 15 h; Inert atmosphere;
参考文献
Clavel; Leger-Lambert; Biran; Serein-Spirau; Bordeau; Roques; Marzouk
Synthesis, 1999 , # 5 p. 829 - 834
反应条件
N,N,N',N',N'',N''-hexamethylphosphoric triamide; samarium diiodide in tetrahydrofuran; benzene Ambient temperature;
参考文献
Yoshida, Masato; Suzuki, Daiki; Iyoda, Masahiko
Journal of the Chemical Society - Perkin Transactions 1, 1997 , # 5 p. 643 - 648
反应条件
Cu-Mg in 10,11-dihydro-5-[3-(methylamino)propyl]-5H-dibenz(b,f)azepin T=25°C; 5 h; Inert atmosphere;
参考文献
Utsumi, Shinya; Katagiri, Toshimasa; Uneyama, Kenji
Tetrahedron, 2012 , vol. 68, # 4 p. 1085 - 1091
反应条件
in tetrahydrofuran; N,N,N',N',N'',N''-hexamethylphosphoric triamide electrochemical reaction;
参考文献
Biran; Bordeau; Bonafoux; Deffieux; Duprat; Jouikov; Leger-Lambert; Moreau; Serein-Spirau
Journal de Chimie Physique et de Physico-Chimie Biologique, 1996 , vol. 93, # 4 p. 591 - 600
反应条件
1: Cu-Mg / 10,11-dihydro-5-[3-(methylamino)propyl]-5H-dibenz(b,f)azepin / 5 h / 25 °C / Inert atmosphere 2: Cu-Mg / 10,11-dihydro-5-[3-(methylamino)propyl]-5H-dibenz(b,f)azepin / 15 h / 25 °C / Inert atmosphere View Scheme
参考文献
Utsumi, Shinya; Katagiri, Toshimasa; Uneyama, Kenji
Tetrahedron, 2012 , vol. 68, # 4 p. 1085 - 1091
反应条件
1: magnesium / 10,11-dihydro-5-[3-(methylamino)propyl]-5H-dibenz(b,f)azepin / 5 h / 25 °C / Inert atmosphere 2: Cu-Mg / 10,11-dihydro-5-[3-(methylamino)propyl]-5H-dibenz(b,f)azepin / 15 h / 25 °C / Inert atmosphere View Scheme
参考文献
Utsumi, Shinya; Katagiri, Toshimasa; Uneyama, Kenji
Tetrahedron, 2012 , vol. 68, # 4 p. 1085 - 1091
反应条件
1: 83 percent / tetrahydrofuran; hexamethylphosphoric acid triamide / electrochemical reaction 2: 52 percent / tetrahydrofuran; hexamethylphosphoric acid triamide / electrochemical reaction View Scheme
参考文献
Biran; Bordeau; Bonafoux; Deffieux; Duprat; Jouikov; Leger-Lambert; Moreau; Serein-Spirau
Journal de Chimie Physique et de Physico-Chimie Biologique, 1996 , vol. 93, # 4 p. 591 - 600
反应条件
in N,N-dimethyl-formamide
参考文献
Guidotti, Jerome; Metz, Francois; Tordeux, Marc; Wakselman, Claude
Synlett, 2004 , # 10 p. 1759 - 1762
