(甲氧基甲基)三甲基硅烷合成路线 (共 16 条)
反应条件
n-butylpotassium in tetrahydrofuran T=-75 - 25°C; butylpotassium was prepared from dibutylmercury;
参考文献
Lehmann, Ruth; Schlosser, Manfred
Tetrahedron Letters, 1984 , vol. 25, # 7 p. 745 - 748
参考文献
Gmelin Handbook: Si: MVol.C, 4, page 14 - 18
Full Text Show Details
Dow Corning Corp.
Patent: GB657443 , 1951 ;
C., 1952 , p. 6435
反应条件
in diethyl ether T=-78°C; Yields of byproduct given;
参考文献
Duchene, Alain; Mouko-Mpegna, David; Quintard, Jean-Paul
Bulletin de la Societe Chimique de France, 1985 , # 5 p. 787 - 793
反应条件
in methanol 19 h; Heating;
参考文献
Tetrahedron Letters, , vol. 26, # 9 p. 1115 - 1118
反应条件
in 1,4-dioxane; methanol 21 h; Heatingvariation of solvents and reaction time; Product distributionMechanism;
参考文献
Tetrahedron Letters, , vol. 26, # 9 p. 1115 - 1118
反应条件
sodium 2.) reflux, 24 h; Yield given. Multistep reaction;
参考文献
Journal of Organometallic Chemistry, , vol. 459, # 1-2 p. 43 - 54
参考文献
Journal of the American Chemical Society, , vol. 70, p. 4142
反应条件
cesium fluoride 1.)-78 deg C, 2.)carefull heating; Product distributionMechanism;
参考文献
Journal of Organic Chemistry, , vol. 49, # 12 p. 2112 - 2116
反应条件
T=65°C; Rate constant;
参考文献
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), , # 12 p. 2411 - 2414
反应条件
T=65°C; Rate constant;
参考文献
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), , # 12 p. 2411 - 2414