反应条件
sulfuric acid in diethyl ether; water (N2); cooling B(OMe)3 in Et2O to -78°C, addn. of the Grignard compd. in Et2O over 2 h, stirring (-78°C, 2 h), warming to room temp., addn. of aq. H2SO4; phase sepn., extn. of the aq. phase (Et2O), evapn. of Et2O, recrystn. from CHCl3 at 55°C; contains some crystal water;
参考文献
Green, Malcolm L. H.; Wagner, Matthias
Journal of the Chemical Society - Dalton Transactions, 1996 , # 12 p. 2467 - 2473
