[(三甲基硅烷基)甲基]膦酸二乙酯合成路线 （共 25 条）
反应条件
N,N-dimethyl-aniline in benzene
参考文献
Liptuga,N.I. et al.
J. Gen. Chem. USSR (Engl. Transl.), 1972 , vol. 42, # 2 p. 293 - 296,284 - 286
反应条件
hydrogenchloride Yield given;
参考文献
Aboujaoude, Elie Elia; Lietje, Stephane; Collignon, Noel; Teulade, Marie Paule; Savignac, Philippe
Synthesis, 1986 , # 11 p. 934 - 937
反应条件
1: 1.) LDA / 1.) THF, hexane, -60 deg C, 10 min, 2.) THF, -70 deg C, 15 min 2: aq. HCl View Scheme
参考文献
Aboujaoude, Elie Elia; Lietje, Stephane; Collignon, Noel; Teulade, Marie Paule; Savignac, Philippe
Synthesis, 1986 , # 11 p. 934 - 937
参考文献
Canavan; Eaborn
Journal of the Chemical Society, 1959 , p. 3751
Full Text Show Details
Gen.Electric Co.
Patent: US2768193 , 1954 ;
Full Text Show Details
Ginsburg; Jakubowitsch
Zhurnal Obshchei Khimii, 1958 , vol. 28, p. 728,732; engl.Ausg.S.710,712,713
反应条件
Yield given. Multistep reaction;
参考文献
Savignac, Philippe; Mathey, Francois
Synthesis, 1982 , # 9 p. 725 - 726
反应条件
1: 1.) n-BuLi / 1.) hexane, THF, -78 deg C, 2.) -78 deg C 2: 1.) n-BuLi / 1.) hexane, THF, -78 deg C, 10 min, 2.) reflux, 30 min View Scheme
参考文献
Mikolajczyk, Marian; Balczewski, Piotr
Synthesis, 1989 , # 2 p. 101 - 106
反应条件
1: 1.) n-BuLi / 1.) hexane, THF, -78 deg C, 2.) -78 deg C 2: 1.) n-BuLi / 1.) hexane, THF, -78 deg C, 20 min, 2.) room temp., 4 h View Scheme
参考文献
Mikolajczyk, Marian; Balczewski, Piotr
Synthesis, 1989 , # 2 p. 101 - 106
反应条件
(i) nBuLi, THF, hexane, (ii) /BRN= 1072099/; Multistep reaction;
参考文献
Carey,F.A.; Court,A.S.
Journal of Organic Chemistry, 1972 , vol. 37, p. 939 - 943
反应条件
cesium fluoride in neat (no solvent)
1.5 h; Irradiation;
参考文献
Latouche, R.; Texier-Boullet, F.; Hamelin, J.
Bulletin de la Societe Chimique de France, 1993 , vol. 130, p. 535 - 546
反应条件
1: 1.) n-BuLi / 1.) hexane, THF, -78 deg C, 2.) -78 deg C
2: 1.) n-BuLi / 1.) hexane, THF, -78 deg C, 20 min, 2.) -78 deg C to 25 deg C
View Scheme
参考文献
Mikolajczyk, Marian; Balczewski, Piotr
Synthesis, 1989 , # 2 p. 101 - 106
