1,4-双(二苯基氨基)苯合成路线 (共 17 条)
反应条件
cesium fluoride; bis(dibenzylideneacetone)-palladium(0); 2-(dicyclohexylphosphino)-2',4',6'-tri-i-propyl-1,1’-biphenyl T=100°C; 3 h; Inert atmosphere;
参考文献
Shimizu, Kenta; Minami, Yasunori; Goto, Osamu; Ikehira, Hideyuki; Hiyama, Tamejiro
Chemistry Letters, 2014 , vol. 43, # 4 p. 438 - 440
反应条件
cesium fluoride; bis(dibenzylideneacetone)-palladium(0); 2-(dicyclohexylphosphino)-2',4',6'-tri-i-propyl-1,1’-biphenyl T=100°C; 14 h; Inert atmosphere;
参考文献
Shimizu, Kenta; Minami, Yasunori; Goto, Osamu; Ikehira, Hideyuki; Hiyama, Tamejiro
Chemistry Letters, 2014 , vol. 43, # 4 p. 438 - 440
反应条件
potassium hydroxide; copper in various solvent(s) T=160°C; 24 h;
参考文献
Paine, Anthony James
Journal of the American Chemical Society, 1987 , vol. 109, # 5 p. 1496 - 1502
反应条件
tri-tert-butyl phosphine; bis(dibenzylideneacetone)-palladium(0); sodium t-butanolate in toluene 1 h; Ambient temperature;
参考文献
Hartwig, John F.; Kawatsura, Motoi; Hauck, Sheila I.; Shaughnessy, Kevin H.; Alcazar-Roman, Luis M.
Journal of Organic Chemistry, 1999 , vol. 64, # 15 p. 5575 - 5580
反应条件
cBRIDP; bis(η3-allyl-μ-chloropalladium(II)); sodium t-butanolate in toluene T=100°C; 3 h; Inert atmosphere;
参考文献
Suzuki, Ken; Hori, Yoji; Kobayashi, Tohru
Advanced Synthesis and Catalysis, 2008 , vol. 350, # 5 p. 652 - 656
反应条件
tris(dibenzylideneacetone)dipalladium(0) chloroform complex; tri-tert-butyl phosphine; sodium t-butanolate; triethylamine in hexane; toluene T=20°C; 4 h;
参考文献
McIlroy, Sean P.; Clo, Emiliano; Nikolajsen, Lars; Frederiksen, Peter K.; Nielsen, Christian B.; Mikkelsen, Kurt V.; Gothelf, Kurt V.; Ogilby, Peter R.
Journal of Organic Chemistry, 2005 , vol. 70, # 4 p. 1134 - 1146
反应条件
potassium carbonate; permethrin in diphenylether T=190°C; Arylation; 24 h;
参考文献
Selby, Trent D.; Stickley, Kurt R.; Blackstock, Silas C.
Organic Letters, 2000 , vol. 2, # 2 p. 171 - 174
反应条件
bis(η3-allyl-μ-chloropalladium(II)); potassium hydroxide in water Buchwald-Hartwig reaction; RefluxInert atmosphere;
参考文献
Hirai, Yoshinori; Uozumi, Yasuhiro
Chemistry - An Asian Journal, 2010 , vol. 5, # 8 p. 1788 - 1795
反应条件
18-crown-6 ether; copper; potassium carbonate in 1,2-dichloro-benzene 24 h; Inert atmosphereReflux;
参考文献
Chung, Yi-Chun; Tu, Yi-Jung; Lu, Shih-Hua; Hsu, Wan-Chi; Chiu, Kuo Yuan; Su, Yuhlong Oliver
Organic Letters, 2011 , vol. 13, # 11 p. 2826 - 2829
反应条件
toluene-4-sulfonic acid in toluene 12 h; Heating;
参考文献
Haga, Kazuo; Iwaya, Katsumasa; Kaneko, Ryohei
Bulletin of the Chemical Society of Japan, 1986 , vol. 59, # 3 p. 803 - 808