Besolova, E. A.; Foss, V. L.; Lutsenko, I. F.
Zhurnal Obshchei Khimii, 1968 , vol. 38, p. 1574 - 1578
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Gmelin Handbook: Sb: Org.Comp.1, 1.1.1.1.3, page 33 - 37
in toluene byproducts: H2; PhOAc added to CoH(N2)(PPh3)3 in toluene in vac., reacted for 2 days at room temp.; liquid phase analysed by GLC; hexane added, ppt. filtered, washed with hexane, dried in vac., recrystd. from C6H6-hexane; elem. anal.;
参考文献
Journal of the American Chemical Society, , vol. 108, # 3 p. 385 - 391
in toluene CH3COOCH2CF3 added to toluene soln. of CoH(N2)(PPh3)3, evacuated, stirred at room temp. for 2 days; hexane added, solid recrystd. from toluene-hexane; elem. anal.;
参考文献
Journal of the American Chemical Society, , vol. 108, # 3 p. 385 - 391
