7-(二苯甲基氧基)-1H-吲哚合成路线 （共 7 条）
反应条件
in tetrahydrofuran T=-40°C; 0.666667 h;
参考文献
Dobson; Todd; Gilmore
Synthetic Communications, 1991 , vol. 21, # 5 p. 611 - 617
反应条件
in tetrahydrofuran T=-40°C;
参考文献
Hirao, Shotaro; Sugiyama, Yumiko; Iwao, Masatomo; Ishibashi, Fumito
Bioscience, Biotechnology and Biochemistry, 2009 , vol. 73, # 8 p. 1764 - 1772
反应条件
1: 87 percent / K2CO3 / dimethylformamide 2: 44 percent / tetrahydrofuran / 1 h / -40 °C View Scheme
参考文献
Journal of the Chemical Society - Perkin Transactions 1, , # 7 p. 1193 - 1202
反应条件
1: 70 percent / K2CO3 / acetone / 5 h / Heating 2: 57 percent / tetrahydrofuran / 0.67 h / -40 °C View Scheme
参考文献
Synthetic Communications, , vol. 21, # 5 p. 611 - 617
反应条件
1: H2 / Pearlman's catalyst / methanol; toluene / 1 h / 2585.7 Torr / Ambient temperature 2: K2CO3 / butan-2-one / 1 h / Heating View Scheme
参考文献
Synthetic Communications, , vol. 21, # 5 p. 611 - 617
反应条件
20 palladium hydroxide on carbon; hydrogen in ethyl acetate T=20°C; 24 h;
参考文献
Hirao, Shotaro; Sugiyama, Yumiko; Iwao, Masatomo; Ishibashi, Fumito
Bioscience, Biotechnology and Biochemistry, 2009 , vol. 73, # 8 p. 1764 - 1772
反应条件
1: hydrogen; palladium on activated charcoal / |Inert atmosphere
2: potassium carbonate / 24 h / 20 °C / |Inert atmosphere
3: sodium cyanoborohydride / acetic acid / |Inert atmosphere
4: N-methyl-formamide / 28 h / 50 °C / |Inert atmosphere
5: 2,3-dicyano-5,6-dichloro-p-benzoquinone / tetrahydrofuran / 0.08 h / |Inert atmosphere
View Scheme
参考文献
Merschaert, Alain; Boquel, Pascal; Van Hoeck, Jean-Pierre; Gorissen, Hugo; Borghese, Alfio; Bonnier, Benjamin; Mockel, Anne; Napora, Freddy
Organic Process Research and Development, 2006 , vol. 10, # 4 p. 776 - 783
