(1S,2S)-(+)-2-甲氧基环己醇合成路线 (共 26 条)
反应条件
TiCl3(OTf) 0.17 h; Heating;
参考文献
Moghadam, Majid; Tangestaninejad, Shahram; Mirkhani, Valiollah; Shaibani, Reza
Tetrahedron, 2004 , vol. 60, # 29 p. 6105 - 6111
反应条件
potassium tert-butylate in water; dimethyl sulfoxide 1 h; Ambient temperature;
参考文献
Hudrlik, Paul F.; Hudrlik, Anne M.; Kulkarni, Ashok K.
Journal of the American Chemical Society, 1982 , vol. 104, # 24 p. 6809 - 6811
反应条件
titanium(III)-tris-(tetrahydridoborate) in dichloromethane T=-20°C; 2 h;
参考文献
Ravikumar; Chandrasekaran, Srinivasan
Tetrahedron, 1997 , vol. 53, # 8 p. 2973 - 2978
反应条件
15percent aqueous acidic TiCl3; 30percent aqueous NH3 in methanol T=0 - 20°C; 0.0833333 h;
参考文献
European Journal of Organic Chemistry, , # 12 p. 2235 - 2243
反应条件
water in methanol T=60°C; P=7500600 Torr; 24 h;
参考文献
Tetrahedron Letters, , vol. 34, # 25 p. 4031 - 4034
反应条件
3-chloro-benzenecarboperoxoic acid in water; tert-butyl alcohol T=20°C; 0.5 h;
参考文献
Cambie, Richard C.; Chambers, David; Lindsay, Barry G.; Rutledge, Peter S.; Woodgate, Paul D.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 822 - 827
反应条件
water T=60°C; P=7500600 Torr; 24 h;
参考文献
Tetrahedron Letters, , vol. 34, # 25 p. 4031 - 4034
反应条件
dihydrogen peroxide; methyltrioxorhenium (VII) T=25°C; 3 h;
参考文献
Chemical Communications, , # 19 p. 1915 - 1916
反应条件
ion-exchange resin lt;OH- formgt;; hydrogen; nickel in methanol P=2585.7 Torr;
参考文献
Canadian Journal of Chemistry, , vol. 45, p. 2605 - 2611
反应条件
ion-exchange resin lt;OH- formgt;; hydrogen; nickel in methanol P=2585.7 Torr;
参考文献
Canadian Journal of Chemistry, , vol. 45, p. 2605 - 2611