1,4-双(三甲基甲硅烷基)苯合成路线 (共 36 条)
反应条件
sodium hydroxide; diphenyl-(o-hydroxyphenyl)-phosphine; PdCl(π-C3H5)2 in tetrahydrofuran T=100°C; Substitution; Silylation; 24 h;
参考文献
Shirakawa; Kurahashi; Yoshida; Hiyama
Chemical Communications, 2000 , # 19 p. 1895 - 1896
参考文献
Gmelin Handbook: Si: MVol.C, 32, page 100 - 103
反应条件
[RhCl(η2:η2-cycloocta-1,5-diene)]2 in 2-cyclohexylethanol T=130°C; 15 h; Inert atmosphere;
参考文献
Journal of the American Chemical Society, , vol. 130, # 47 p. 15982 - 15989
反应条件
[RhCl(η2:η2-cycloocta-1,5-diene)]2 in 2-cyclohexylethanol T=130°C; 15 h; Inert atmosphere;
参考文献
Journal of the American Chemical Society, , vol. 130, # 47 p. 15982 - 15989
反应条件
di-tert-butyl peroxide T=130°C; 6.5 h;
参考文献
Chemistry Letters, , p. 599 - 602
参考文献
Gmelin Handbook: Si: MVol.C, 32, page 100 - 103
反应条件
sodium methylate in N,N,N',N',N'',N''-hexamethylphosphoric triamide
参考文献
Organic letters, , vol. 3, # 8 p. 1197 - 1200
反应条件
chloro-trimethyl-silane; magnesium in tetrahydrofuran Heating;
参考文献
Kaim, Wolfgang; Tesmann, Holger; Bock, Hans
Chemische Berichte, 1980 , vol. 113, # 10 p. 3221 - 3234
反应条件
di-tert-butyl peroxide T=0°C; 3.5 h; Irradiation;
参考文献
Chemistry Letters, , p. 599 - 602
反应条件
1: n-BuLi / hexane; pentane; diethyl ether / 48 h 2: 90 percent View Scheme
参考文献
European Journal of Inorganic Chemistry, , # 6 p. 761 - 769