2,2-二甲基-1,3-丙二醇合成路线 （共 467 条）
反应条件
in chloroform-d1 T=20°C; 0.75 h; Title compound not separated from byproducts.;
参考文献
Roy, Chandra D.; Brown, Herbert C.
Monatshefte fur Chemie, 2007 , vol. 138, # 9 p. 879 - 887
参考文献
Meyersberg
Monatshefte fuer Chemie, 1905 , vol. 26, p. 43 Anm.3
参考文献
Kita, Yusuke; Tobisu, Mamoru; Chatani, Naoto
Organic Letters, 2010 , vol. 12, # 8 p. 1864 - 1867
反应条件
Novozyme 435 in 1,1-dimethylpropan-1-ol T=50°C; 120 h; Inert atmosphereMolecular sieveEnzymatic reaction;
参考文献
Popescu, Dragos; Hoogenboom, Richard; Keul, Helmut; Moeller, Martin
Journal of Polymer Science, Part A: Polymer Chemistry, 2010 , vol. 48, # 12 p. 2610 - 2621
反应条件
in tetrahydrofuran T=20°C; 0.166667 h;
参考文献
Journal of the Chemical Society. Perkin Transactions 1, , # 11 p. 1397 - 1400
反应条件
1: 2-((2-(methoxy)ethoxy)methoxy)-1,1,1-trifluoroethane With lithium diisopropyl amide in tetrahydrofuran; hexane T=-78 - -65°C; 2.5 h; Inert atmosphere; 2: With tri-isopropoxy-borane in tetrahydrofuran; hexane T=-65 - -30°C; 4 h; Inert atmosphere; 3: 3-hydroxy-2,2-dimethylpropanol Further stages;
参考文献
Katz, Jason D.; Lapointe, Blair T.; Dinsmore, Christopher J.
Journal of Organic Chemistry, 2009 , vol. 74, # 22 p. 8866 - 8869
反应条件
acyl transferase from Mycobacterium smegmatis in aq. phosphate buffer T=20°C; pH=8; 0.5 h; Enzymatic reaction;
参考文献
Wiermans, Lotte; Hofzumahaus, Sebastian; Schotten, Christiane; Weigand, Lisa; Schallmey, Marcus; Schallmey, Anett; De Maria, Pablo Dominguez
ChemCatChem, 2013 , vol. 5, # 12 p. 3719 - 3724
反应条件
acyl transferase from Mycobacterium smegmatis in aq. phosphate buffer T=20°C; pH=8; 0.5 h; Enzymatic reaction; ConcentrationpH-valueTime;
参考文献
Wiermans, Lotte; Hofzumahaus, Sebastian; Schotten, Christiane; Weigand, Lisa; Schallmey, Marcus; Schallmey, Anett; De Maria, Pablo Dominguez
ChemCatChem, 2013 , vol. 5, # 12 p. 3719 - 3724
反应条件
1: phosphorus trichoride; triethylamine / diethyl ether / 2 h / 0 °C / |Inert atmosphere 2: triethylamine / tetrahydrofuran / 1 h / |Inert atmosphere; |Reflux View Scheme
参考文献
Salah, Nessrine; Arfaoui, Youssef; Bahri, Mohamed; Efrit, Mohamed Lotfi; Akacha, Azaiez Ben
Phosphorus, Sulfur and Silicon and the Related Elements, 2013 , vol. 188, # 5 p. 609 - 622
反应条件
N-ethyl-N,N-diisopropylamine in tetrahydrofuran T=20°C; 12 h;
参考文献
Organic Letters, , vol. 10, # 8 p. 1565 - 1568
