3-苯基-2-丙烯醛2-(2,4-二硝基苯基)腙合成路线 (共 8 条)
反应条件
1: cinnamic alcohol With C93H73Br4N3O2P4Ru2; oxygen in dichloromethane T=20°C; P=760.051 Torr; 6 h; 2: (2,4-dinitro-phenyl)-hydrazine
参考文献
Manimaran, Arumugam; Jayabalakrishnan, Chinnasamy
Synthesis and Reactivity in Inorganic, Metal-Organic and Nano-Metal Chemistry, 2010 , vol. 40, # 2 p. 116 - 128
反应条件
oxidized single-walled carbon nanotubes(SWCNs-COOH) in ethanol T=80°C; 0.75 h;
参考文献
Borazjani, Maryam Kiani; Safaei, Hamid Reza; Panahandeh, Majid; Kiani, Ali Reza; Kiani, Masoumeh; Mofarahi, Masoud
South African Journal of Chemistry, 2013 , vol. 66, p. 279 - 281
反应条件
hydrogenchloride; diethylene glycol dimethyl ether stereoisomer(ic) of mp: 260 degree;
参考文献
Johnson
Journal of the American Chemical Society, 1953 , vol. 75, p. 2720,2721
Journal of the American Chemical Society, 1951 , vol. 73, p. 5888
反应条件
iron (III) perchlorate in 1,2-dichloro-ethane T=20°C; 32 h;
参考文献
Oskooie, Hossien A.; Heravi, Majid M.; Sadnia, Akbar; Safarzadegan, Mehrak; Behbahani, Farahnaz K.
Mendeleev Communications, 2007 , vol. 17, # 3 p. 190 - 191
反应条件
1: tert.-butylhydroperoxide; C24H28Cl2FeN6O2*ClH / methanol / 15 h / 50 - 60 °C 2: methanol View Scheme
参考文献
Ahuja, Gauri; Mathur, Pavan
Spectrochimica Acta - Part A: Molecular and Biomolecular Spectroscopy, 2011 , vol. 83, # 1 p. 180 - 186
反应条件
1: alcohol; hydrazine hydrate 2: acetic acid View Scheme
参考文献
Purgotti
Gazzetta Chimica Italiana, 1894 , vol. 24 I, p. 568
反应条件
sulfuric acid stereoisomer(ic) of mp: 260 degree;
参考文献
Braude; Forbes
Journal of the Chemical Society, 1951 , p. 1755,1760
反应条件
stereoisomer(ic) of mp: 260 degree;
参考文献
Gen. Aniline and Film Corp.
Patent: US2677707 , 1950 ;