5-甲基-1,3-二乙氰基苯合成路线 (共 8 条)
反应条件
tetrabutylammomium bromide in dichloromethane; water 8 - 9 h; Heating / reflux;
参考文献
US2006/189670 A1, ;
Page/Page column 5-6 ;
反应条件
tetrabutylammomium bromide in dichloromethane; water
参考文献
US4935437 A1, ;
US 4935437 A
反应条件
tetrabutylammomium bromide in dichloromethane; water 16 h; Heating;
参考文献
Organic and Biomolecular Chemistry, , vol. 5, # 18 p. 2940 - 2952
反应条件
18-crown-6 ether in acetonitrile 18 h; Reflux;
参考文献
Journal of Medicinal Chemistry, , vol. 51, # 11 p. 3154 - 3170
参考文献
Chemische Berichte, , vol. 58, p. 283
参考文献
Chemische Berichte, , vol. 58, p. 283
反应条件
sodium hydride in N,N-dimethyl-formamide T=20°C; 12 h;
参考文献
Jackson, Toby; Woo, L. W. Lawrence; Trusselle, Melanie N.; Chander, Surinder K.; Purohit, Atul; Reed, Michael J.; Potter, Barry V. L.
Organic and Biomolecular Chemistry, 2007 , vol. 5, # 18 p. 2940 - 2952
反应条件
sodium hydride in N,N-dimethyl-formamide T=0°C; Inert atmosphere;
参考文献
Mei, Yu-Hua; Luo, Yu; Lu, Wei
Organic Preparations and Procedures International, 2008 , vol. 40, # 5 p. 487 - 489