N-羟甲基邻苯二甲酰亚胺合成路线 (共 74 条)
反应条件
sodium methylate 1.) electrolysis, current density 0.05 A/cm2, 1.5 h, 2.) electrolysis, current density 0.02 A/cm2, 5 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Tetrahedron, , vol. 54, # 26 p. 7517 - 7524
反应条件
sodium methylate 1.) electrolysis, current density 0.05 A/cm2, 2 h, 2.) electrolysis, current density 0.02 A/cm2, 5 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Tetrahedron, , vol. 54, # 26 p. 7517 - 7524
反应条件
1: bromine / 160 - 170 °C 2: water View Scheme
参考文献
Chemische Berichte, , vol. 31, p. 1229
反应条件
in benzene 12 h; Heating; Title compound not separated from byproducts;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 93 - 96
反应条件
15 h; UV-irradiation;
参考文献
Sinderhauf, Katrin; Schwack, Wolfgang
Journal of Agricultural and Food Chemistry, 2003 , vol. 51, # 20 p. 5990 - 5995
参考文献
Chemische Berichte, , vol. 31, p. 3234
DE104624 ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 5, p. 926
反应条件
in methanol 7 h; UV-irradiation; Product distribution; Further Variations:Solvents;
参考文献
Journal of Agricultural and Food Chemistry, , vol. 51, # 20 p. 5990 - 5995
参考文献
Chemische Berichte, , vol. 31, p. 1229
反应条件
sulfuric acid T=0°C;
参考文献
Smythe; Von Itzstein
Journal of the American Chemical Society, 1994 , vol. 116, # 7 p. 2725 - 2733
反应条件
1: 80 percent / PBr3 / 1 h / 140 °C 2: 81 percent / 1 h / 120 °C View Scheme
参考文献
Hirschmann, Ralph; Yager, Kraig M.; Taylor, Carol M.; Witherington, Jason; Sprengeler, Paul A.; Phillips, Barton W.; Moore, William; Smith III, Amos B.
Journal of the American Chemical Society, 1997 , vol. 119, # 35 p. 8177 - 8190