反应条件
1: 85 percent / 1.) nBuLi / tetrahydrofuran; hexane / 1.) N2 atm., -78 degC, 15 min; 2.) -78 degC, 1 h then r.t., 1 h 2: 82 percent / HgCl2, HgO / acetone; H2O / 2 h / Heating 3: 95 percent / LiAlH4 / diethyl ether / 3 h / Heating View Scheme
参考文献
Bulletin of the Chemical Society of Japan, , vol. 62, # 6 p. 2013 - 2017