2,2,6,6-四甲基-3,5-庚二酮合成路线 （共 42 条）
反应条件
potassium tert-butylate in N,N-dimethyl-formamide T=50°C; 5 h;
参考文献
Nandurkar, Nitin S.; Bhanushali, Mayur J.; Patil, Dinkar S.; Bhanage, Bhalchandra M.
Synthetic Communications, 2007 , vol. 37, # 23 p. 4111 - 4115
反应条件
1: benzene; magnesium 2: diethyl ether; sodium amide View Scheme
参考文献
Journal of the American Chemical Society, , vol. 73, p. 901
反应条件
diethyl ether; sodium amide
参考文献
Journal of the American Chemical Society, , vol. 73, p. 901
反应条件
diethyl ether; sodium amide
参考文献
Journal of the American Chemical Society, , vol. 78, p. 6066,6069
反应条件
in diethyl ether; toluene T=0°C; 24 h; Inert atmosphere;
参考文献
Molecules, , vol. 17, # 6 p. 6415 - 6423
反应条件
hydrogenchloride; triethylamine 1.) acetonitrile, reflux, 18 h, 2.) ethanol, reflux, 20 h; Yield given. Multistep reaction;
参考文献
Australian Journal of Chemistry, , vol. 37, # 7 p. 1453 - 1460
反应条件
in methanol Kinetics; 9-hydroxyquinoline, methanol, 298 K; detected by UV spectra;
参考文献
Inorganica Chimica Acta, , vol. 342, p. 97 - 106
反应条件
in methanol Kinetics; byproducts: methanol; 9-hydroxyquinoline, methanol, 298 K; detected by UV spectra;
参考文献
Inorganica Chimica Acta, , vol. 342, p. 97 - 106
反应条件
24 h; Heating; Title compound not separated from byproducts;
参考文献
Kollenz, Gert; Kappe, C. Olivier; Nabey, Hesham Abd el
Heterocycles, 1991 , vol. 32, # 4 p. 669 - 673
反应条件
sodium amide 1.) ether, 20 deg C, 2.) ether, a) 20 deg C, 1 h, b) 35 deg C, 2 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Bull. Russ. Acad. Sci. Div. Chem. Sci. (Engl. Transl.), , vol. 41, # 7.2 p. 1591 - 1601,1227 - 1234
