1,3-二氯-2,2-二氟丙烷合成路线 （共 14 条）
反应条件
Liefert beim Chlorieren im Sonnenlicht erst 2.2-Difluor-1.1.3-trichlor-propan, dann 2.2-Difluor-1.1.1.3-tetrachlor-propan und zuletzt;
参考文献
Henne; Flanagan
Journal of the American Chemical Society, 1943 , vol. 65, p. 2362
反应条件
hydrogen fluoride; mercury(II) oxide
T=125°C;
参考文献
Henne; Flanagan
Journal of the American Chemical Society, 1943 , vol. 65, p. 2362
反应条件
bromine trifluoride in 1,2,2-trifluoro-trichloroethane
T=10 - 20°C;
参考文献
Boguslavskaya, L. S.; Chuvatkin, N. N.; Kartashov, A. V.; Ternovskoi, L. A.
Journal of Organic Chemistry USSR (English Translation), 1987 , vol. 23, p. 230 - 236
Zhurnal Organicheskoi Khimii, 1987 , vol. 23, # 2 p. 262 - 269
反应条件
sulfur(IV) fluoride
T=120 - 130°C; 3 h;
参考文献
Wielgat,J.; Domagala,Z.; Kolinski,R.
Journal of Fluorine Chemistry, 1987 , vol. 35, p. 643
反应条件
phosphorus pentachloride
T=150 - 170°C;
参考文献
Boguslavskaya,L.S. et al.
Journal of Organic Chemistry USSR (English Translation), 1971 , vol. 7, p. 1382 - 1387
Zhurnal Organicheskoi Khimii, 1971 , vol. 7, # 7 p. 1338 - 1343
反应条件
fluoro chloride
T=-120 - 20°C; 16 h;
参考文献
Arimura, Takashi; Kurosawa, Shigeru; Sekiya, Akira
Chemistry Letters, 1993 , # 1 p. 35 - 36
反应条件
fluoro chloride
T=-120 - -10°C; 12 h; Further byproducts given. Title compound not separated from byproducts;
参考文献
Arimura, Takashi; Kurosawa, Shigeru; Sekiya, Akira
Chemistry Letters, 1993 , # 1 p. 35 - 36
反应条件
fluoro chloride
T=-120 - -10°C; 12 h; Further byproducts given. Title compound not separated from byproducts;
参考文献
Arimura, Takashi; Kurosawa, Shigeru; Sekiya, Akira
Chemistry Letters, 1993 , # 1 p. 35 - 36
反应条件
sulfur(IV) fluoride
T=120 - 130°C; 3 h; Further byproducts given;
参考文献
Wielgat,J.; Domagala,Z.; Kolinski,R.
Journal of Fluorine Chemistry, 1987 , vol. 35, p. 643
反应条件
sulfur(IV) fluoride; hydrogen fluoride
Yield given. Yields of byproduct given;
参考文献
Wielgat, Jerzy; Domagala, Zdzislaw; Kolinski, Ryszard A.
Journal of Fluorine Chemistry, 1985 , vol. 29, p. 182
