potassium dichromate; N-benzyl-N,N,N-triethylammonium chloride in N,N,N',N',N'',N''-hexamethylphosphoric triamide T=112 - 120°C; 4 h; Title compound not separated from byproducts;
potassium dichromate; N-benzyl-N,N,N-triethylammonium chloride in N,N,N',N',N'',N''-hexamethylphosphoric triamide T=110 - 120°C; 14 h; Title compound not separated from byproducts;
hydrogen; palladium on activated charcoal T=20°C; 24 h; atmospheric pressure;
参考文献
Fujii, Yasuyuki; Furugaki, Hisakazu; Tamura, Eiko; Yano, Shinji; Kita, Katsumi
Bulletin of the Chemical Society of Japan, 2005 , vol. 78, # 3 p. 456 - 463