1: thiophenol With sodium hydride in N,N-dimethyl-formamide; mineral oil T=25°C; 1 h; Inert atmosphere; 2: 2-chloro-3-pyridinecarbonitrile in N,N-dimethyl-formamide; mineral oil T=25°C; 16 h; Inert atmosphere;
参考文献
Melzig, Laurin; Metzger, Albrecht; Knochel, Paul
Chemistry - A European Journal, 2011 , vol. 17, # 10 p. 2948 - 2956
sodium hydroxide; sodium chloride in water T=298°C; also investigated: Rk. without phenol, rk. without NaCl, and rk. without thiophenol (NaOPh instead of PhOH); other temp.; MechanismProduct distribution;
参考文献
Journal of Organic Chemistry, , vol. 45, # 10 p. 1776 - 1782