5-乙烯基-5-甲基四氢呋喃-2-酮合成路线 （共 8 条）
反应条件
pyridinium chlorochromate in dichloromethane T=28°C; 2 h; celite;
参考文献
Baskaran, S.; Islam, I.; Raghavan, Malini; Chandrasekaran, S.
Chemistry Letters, 1987 , p. 1175 - 1178
反应条件
3 A molecular sieve; pyridinium chlorochromate in dichloromethane 3 h; Heating;
参考文献
Baskaran, Sundarababu; Islam, Imadul; Chandrasekaran, Srinivasan
Journal of Chemical Research, Miniprint, 1992 , p. 2213 - 2246
反应条件
in tetrahydrofuran 2 h;
参考文献
Mazzini, Francesco; Galli, Francesco; Salvadori, Piero
European Journal of Organic Chemistry, 2006 , # 24 p. 5588 - 5593
反应条件
1: 72 percent / m-chloroperbenzoic acid / CHCl3 / 8 h / 0 °C 2: 73 percent / pyridinium chlorochromate, molecular sieves 3 Angstroem / CH2Cl2 / 4 h / Heating View Scheme
参考文献
Baskaran, Sundarababu; Islam, Imadul; Chandrasekaran, Srinivasan
Journal of Organic Chemistry, 1990 , vol. 55, # 3 p. 891 - 895
反应条件
1: 96 percent / potassium tert-butoxide / tetrahydrofuran; 2-methyl-propan-2-ol / 1 h / 50 - 60 °C 2: 90 percent / pyridinium chlorochromate / CH2Cl2 / 2 h / 28 °C / celite View Scheme
参考文献
Baskaran, Sundarababu; Islam, Imadul; Chandrasekaran, Srinivasan
Journal of Organic Chemistry, 1990 , vol. 55, # 3 p. 891 - 895
反应条件
in tetrahydrofuran; benzene T=0°C; 2 h;
参考文献
Citron, Christian A.; Rabe, Patrick; Dickschat, Jeroen S.
Journal of Natural Products, 2012 , vol. 75, # 10 p. 1765 - 1776
反应条件
1: 65 percent / Me3OBF4 / CH2Cl2 / 71 h / Ambient temperature 2: 100 mg / diisobutylaluminum hydride / toluene; tetrahydrofuran / 2.7 h / -78 °C 3: diethyl ether / 3 h / Ambient temperature View Scheme
参考文献
Bulletin of the Chemical Society of Japan, , vol. 61, # 11 p. 4051 - 4056
反应条件
hydrogenchloride; zinc(II) chloride in 1,4-dioxane
2 h; Heating;
参考文献
Mazzini, Francesco; Galli, Francesco; Salvadori, Piero
European Journal of Organic Chemistry, 2006 , # 24 p. 5588 - 5593
