(1R,2R)-反-1,2-环己二醇合成路线 (共 93 条)
反应条件
tungsten(VI) oxide dihydrate; phosphoric acid; dihydrogen peroxide in water T=70°C; 3 h;
参考文献
Antonetti, Claudia; Galletti, Anna Maria Raspolli; Accorinti, Pasquale; Alini, Stefano; Babini, Pierpaolo; Raabova, Katerina; Rozhko, Elena; Caldarelli, Aurora; Righi, Paolo; Cavani, Fabrizio; Concepcion, Patricia
Applied Catalysis A: General, 2013 , vol. 466, p. 21 - 31
反应条件
trislt;trinitratocerium(IV)gt; paraperiodate; water in acetonitrile 1 h; Ambient temperature;
参考文献
Iranpoor; Zardaloo
Synthetic Communications, 1994 , vol. 24, # 14 p. 1959 - 1969
反应条件
tungsten(VI) oxide dihydrate; phosphoric acid; dihydrogen peroxide in water T=70°C; 3 h;
参考文献
Antonetti, Claudia; Galletti, Anna Maria Raspolli; Accorinti, Pasquale; Alini, Stefano; Babini, Pierpaolo; Raabova, Katerina; Rozhko, Elena; Caldarelli, Aurora; Righi, Paolo; Cavani, Fabrizio; Concepcion, Patricia
Applied Catalysis A: General, 2013 , vol. 466, p. 21 - 31
反应条件
C46H50CoF6N6O4; water; toluene-4-sulfonic acid in tert-butyl methyl ether T=23°C; 45 h; optical yield given as percent ee;
参考文献
Park, Jongwoo; Lang, Kai; Abboud, Khalil A.; Hong, Sukwon
Chemistry - A European Journal, 2011 , vol. 17, # 7 p. 2236 - 2245
反应条件
1: With (5aS,10bR)-9-nitro-2-phenyl-4,5a,6,10b-tetrahydroindeno[2,1-b][1,2,4]triazolo[4,3-d][1,4]oxazin-2-ium tetrafluoroborate; 4-(N,N-dimethylamino)benzoic acid; N,N,N',N'-tetra-methylnaphthalene-1,8-diamine in chloroform T=20°C; 0.166667 h; 2: With 2-bromo-3-phenylpropanal in chloroform T=0°C; 15 h; Reagent/catalyst;
参考文献
Kuwano, Satoru; Harada, Shingo; Kang, Bubwoong; Oriez, Raphael; Yamaoka, Yousuke; Takasu, Kiyosei; Yamada, Ken-Ichi
Journal of the American Chemical Society, 2013 , vol. 135, # 31 p. 11485 - 11488
反应条件
(S,S)-bis(4-benzyl-4,5-dihydrooxazol-4-yl)methylamine; N-ethyl-N,N-diisopropylamine; copper dichloride in dichloromethane T=0°C; 2 h; Title compound not separated from byproducts;
参考文献
Organic Letters, , vol. 7, # 12 p. 2325 - 2328
反应条件
hydrogen; toluene-4-sulfonic acid; palladium on activated charcoal in 1,4-dioxane T=20°C; 4.5 h;
参考文献
Hirose, Keiji; Aksharanandana, Pakatip; Suzuki, Michiko; Wada, Kiyoshi; Naemura, Koichiro; Tobe, Yoshito
Heterocycles, 2005 , vol. 66, # 1 p. 405 - 431
反应条件
ammonium cerium(IV) nitrate; water in acetonitrile T=0°C; Hydrolysis; 0.666667 h;
参考文献
Journal of the American Chemical Society, , vol. 122, # 10 p. 2252 - 2260
反应条件
ammonium cerium(IV) nitrate; water in acetonitrile T=0°C; 0.666667 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Angewandte Chemie - International Edition, , vol. 37, # 16 p. 2223 - 2226
反应条件
sodium tetrahydroborate in methanol T=0°C; 0.333333 h;
参考文献
Hayashi, Yujiro; Yamaguchi, Junichiro; Sumiya, Tatsunobu; Hibino, Kazuhiro; Shoji, Mitsuru
Journal of Organic Chemistry, 2004 , vol. 69, # 18 p. 5966 - 5973