(二甲氨基亚甲基)二甲基氯化铵合成路线 （共 34 条）
反应条件
1: oxalyl dichloride / tetrahydrofuran / 20 - 40 °C 2: iodine; magnesium / acetonitrile / 6 h / Reflux View Scheme
参考文献
BOEHRINGER INGELHEIM INTERNATIONAL GMBH; FADER, Lee; BEAULIEU, Pierre Louis; BAILEY, Murray; BILODEAU, François; CARSON, Rebekah; GIROUX, André; GODBOUT, Cédrickx; HUCKE, Oliver; JOLY, Marc-André; LEBLANC, Mélissa; LEPAGE, Olivier; MOREAU, Benoît; NAUD, Julie; POIRIER, Martin; VILLEMURE, Elisia
Patent: WO2013/152065 A2, 2013 ;
Location in patent: Page/Page column 51; 52 ;
反应条件
chloro-trimethyl-silane in acetonitrile T=20°C; 24 h;
参考文献
Schroth, Werner; Jahn, Ullrich; Stroehl, Dieter
Chemische Berichte, 1994 , vol. 127, # 10 p. 2013 - 2022
参考文献
Bestmann, Hans Juergen; Schmid, Guenter; Oechsner, Helmut; Ermann, Peter
Chemische Berichte, 1984 , vol. 117, # 4 p. 1561 - 1571
反应条件
chloro-trimethyl-silane in acetonitrile T=20°C; 170 h;
参考文献
Schroth, Werner; Jahn, Ullrich; Stroehl, Dieter
Chemische Berichte, 1994 , vol. 127, # 10 p. 2013 - 2022
反应条件
2,5,6-Trichlor-1,3-benzodioxo in toluene 3 h; Heating; Yield given;
参考文献
Costisella, Burkhard; Gross, Hans
Phosphorus and Sulfur and the Related Elements, 1980 , vol. 8, p. 99 - 104
反应条件
tetrachloromethane in diethyl ether T=20°C; 48 h;
参考文献
Shevchenko, I. V.; Furmanova, M. V.; Kukhar', V. P.; Kolodyazhnyi, O. I.
J. Gen. Chem. USSR (Engl. Transl.), 1989 , vol. 59, # 10.1 p. 2206 - 2211,1977 - 1981
反应条件
iodine; magnesium in ethylene glycol dimethyl ether 24 h; Reflux;
参考文献
Kantlehner, Willi; Aichholz, Reiner; Karl, Martin
Zeitschrift fur Naturforschung - Section B Journal of Chemical Sciences, 2012 , vol. 67, # 4 p. 305 - 319
参考文献
Toeniskoetter,R.H.; Killip,K.A.
Journal of the American Chemical Society, 1964 , vol. 86, p. 690 - 694
反应条件
in diethyl ether 10 h;
参考文献
Shevchenko, I. V.; Furmanova, M. V.; Kukhar', V. P.; Kolodyazhnyi, O. I.
J. Gen. Chem. USSR (Engl. Transl.), 1989 , vol. 59, # 10.1 p. 2206 - 2211,1977 - 1981
反应条件
iodine; magnesium in acetonitrile 6 h; Reflux;
参考文献
Kantlehner, Willi; Aichholz, Reiner; Karl, Martin
Zeitschrift fur Naturforschung - Section B Journal of Chemical Sciences, 2012 , vol. 67, # 4 p. 305 - 319
