4-(1,3-二硫烷-2-基)苯甲腈合成路线 (共 5 条)
反应条件
amberlyst-15 in acetonitrile 1 h;
参考文献
Wiles, Charlotte; Watts, Paul; Haswell, Stephen J.
Tetrahedron Letters, 2007 , vol. 48, # 41 p. 7362 - 7365
反应条件
2,4,6-trichloro-1,3,5-triazine in N,N-dimethyl-formamide T=20°C; 0.5 h;
参考文献
Bandgar, Babasaheb P.; Joshi, Neeta S.; Bettigeri, Sampada V.
Monatshefte fur Chemie, 2007 , vol. 138, # 1 p. 67 - 71
反应条件
1: With copper(l) iodide in chloroform T=20°C; 0.166667 h; 2: With 2,3-dicyano-5,6-dichloro-p-benzoquinone in chloroform 1 h; 3: With water in chloroform T=20°C; 21 h;
参考文献
Fu, Liang; Yao, Chang-Jiang; Chang, Ning-Jie; Chen, Jia-Rong; Lu, Liang-Qiu; Xiao, Wen-Jing
Organic and Biomolecular Chemistry, 2012 , vol. 10, # 3 p. 506 - 508
反应条件
TeCl4 in dichloromethane Ambient temperature;
参考文献
Oksdath-Mansilla, Gabriela; Penenory, Alicia B.
Tetrahedron Letters, 2007 , vol. 48, # 35 p. 6150 - 6154
反应条件
diisobutylaluminium hydride in hexane; benzene
0.5 h;
参考文献
Lindsey, Jonathan S.; Schreiman, Irwin C.; Hsu, Henry C.; Kearney, Patrick C.; Marguerettaz, Anne M.
Journal of Organic Chemistry, 1987 , vol. 52, # 5 p. 827 - 836