1-氯-4-(三甲基甲硅烷基)苯合成路线 （共 29 条）
反应条件
1: 1-chloro-4-bromobenzene With n-butyllithium in tetrahydrofuran; hexane T=-78°C; 1 h; 2: chloro-trimethyl-silane in tetrahydrofuran; hexane T=-78 - 20°C;
参考文献
Ball, Liam T.; Lloyd-Jones, Guy C.; Russell, Christopher A.
Chemistry - A European Journal, 2012 , vol. 18, # 10 p. 2931 - 2937
参考文献
Burkhard
Journal of the American Chemical Society, 1946 , vol. 68, p. 2103
Full Text View citing articles Show Details
Gmelin Handbook: Si: MVol.C, 22, page 68 - 71
反应条件
sodium methylate in N,N,N',N',N'',N''-hexamethylphosphoric triamide
参考文献
Organic letters, , vol. 3, # 8 p. 1197 - 1200
参考文献
Chvalovsky, V.; Bazant, V.
Collection of Czechoslovak Chemical Communications, 1951 , vol. 16, p. 580 - 590
Full Text Show Details
Gmelin Handbook: Si: MVol.C, 22, page 68 - 71
反应条件
1: 1-chloro-4-bromobenzene With n-butyllithium in tetrahydrofuran; cyclohexane T=20 - 22°C; Inert atmosphere; 2: chloro-trimethyl-silane in tetrahydrofuran; cyclohexane T=20 - 22°C; 0.25 h; Inert atmosphere;
参考文献
Tetrahedron Letters, , vol. 51, # 37 p. 4793 - 4796
反应条件
in N,N,N',N',N'',N''-hexamethylphosphoric triamide 0.5 h;
参考文献
Journal of Physical Organic Chemistry, , vol. 15, # 12 p. 889 - 893
反应条件
iodine; magnesium in diethyl ether 18 h; Heating; Title compound not separated from byproducts;
参考文献
Journal of Organometallic Chemistry, , vol. 216, # 3 p. 281 - 286
反应条件
tetrakis(triphenylphosphine) palladium(0) in toluene byproducts: Bu3SnBr, Me3SiBr; at 115°C for 15 h in sealed thick wall Pyrex glass ampoules;
参考文献
Journal of Organometallic Chemistry, , vol. 215, # 1 p. 49 - 58
反应条件
magnesium in N,N,N',N',N'',N''-hexamethylphosphoric triamide
参考文献
Liebigs Annalen der Chemie, , p. 842 - 857
反应条件
magnesium dann mit Chlor-trimethyl-silan;
