反应条件
in chlorobenzene mixt. refluxed in a Soxhlet extraction app. under N2, extractor thimble charged with oven-dried Na2CO3 and sand in a 3:1 ratio, complete after 17 h; monitored by HPLC; evapd. (vac.), column chromy. (silica, MeOH), evapd.; elem. anal.;
参考文献
Doyle, Michael P.; Westrum, Larry J.; Wolthuis, Wendelmoed N. E.; See, Marjorie M.; Boone, William P.; Bagheri, Vahid; Pearson, Matthew M.
Journal of the American Chemical Society, 1993 , vol. 115, # 3 p. 958 - 964