1,3-丙酮二羧酸二乙酯合成路线 （共 169 条）
反应条件
1: With chlorosulfonic acid in dichloromethane T=5°C; 5 h; 2: in ethanol T=0 - 35°C; 2 h;
参考文献
Poldy, Jacqueline; Barrow, Russell A.; Peakall, Rod
European Journal of Organic Chemistry, 2012 , # 29 p. 5818 - 5827,10
反应条件
1: citric acid With chlorosulfonic acid in dichloromethane T=5°C; 5 h; 2: ethanol in dichloromethane T=0 - 35°C; 2 h;
参考文献
Poldy, Jacqueline; Peakall, Rod; Barrow, Russell A.
European Journal of Organic Chemistry, 2012 , # 29 p. 5818 - 5827
参考文献
Justus Liebigs Annalen der Chemie, , vol. 422, p. 11
Journal of the Chemical Society, , vol. 121, p. 1644
Organic Syntheses 5 <New York 1925>, S. 53
参考文献
Justus Liebigs Annalen der Chemie, , vol. 422, p. 11
Journal of the Chemical Society, , vol. 121, p. 1644
反应条件
chloroform T=0°C; Erwaermen des Reaktionsgemisches mit Aethanol.;
参考文献
Collection of Czechoslovak Chemical Communications, , vol. 19, p. 1231,1236
反应条件
1: 95percent sulfuric acid / 1 h 20 deg C, then 3 h 50 deg C 2: H2SO4 / H2O; CHCl3 / 1 h / 35 - 40 °C View Scheme
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 24, p. 101 - 104
Zhurnal Organicheskoi Khimii, , vol. 24, # 1 p. 116 - 119
反应条件
1: oxalic acid diethyl ester With sodium ethanolate 2: acetone
参考文献
Organic Letters, , vol. 13, # 12 p. 3194 - 3197
反应条件
boron trifluoride diethyl etherate; water 1.) ethanol, reflux, 48 h; Yield given. Multistep reaction;
参考文献
Synthesis, , # 2 p. 130 - 133
参考文献
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, , vol. 111, p. 683
Chemische Berichte, 24 Ref. <1891>, 38
