Yamamoto, Yoshinori; Yamamoto, Shinichi; Yatagai, Hidetaka; Maruyama, Kazuhiro
Journal of the American Chemical Society, 1980 , vol. 102, # 7 p. 2318 - 2325
1: sodium carbonate; acetic acid / dichloromethane; water / 6 h / 15 - 25 °C
2: sodium hydroxide; tri-n-butylmethylammonium chloride / water / 4 h / 60 °C / |Large scale
3: triethylamine / ethyl acetate / 0.42 h / -15 °C
4: triethylamine / ethyl acetate / 0.25 h / -15 °C
5: hydrogenchloride / water; ethyl acetate / 0.5 h / 15 - 25 °C
6: sodium hydroxide; tri-n-butylmethylammonium chloride / water / 2 h / 20 - 25 °C / |Large scale
7: ammonium hydroxide / methanol / 3 h / 40 °C / |Large scale
8: dichloromethane; isopropyl alcohol / 5 h / |Large scale
View Scheme
参考文献
Henegar, Kevin E.; Ball, Cynthia T.; Horvath, Carolyn M.; Maisto, Keith D.; Mancini, Sarah E.
Organic Process Research and Development, 2007 , vol. 11, # 3 p. 346 - 353
