反应条件
1: 99 percent / 1) sec-butyllithium / tetrahydrofuran / 1.) -78 deg C, 0.5 h, 2.) RT, 1 h 2: m-chloroperoxybenzoic acid / CH2Cl2 / 1.)0 deg C, 15 min, 2.) RT, 6 h 3: aq. H2SO4 / methanol / 1 h / Ambient temperature View Scheme
参考文献
Synthetic Communications, , vol. 13, # 12 p. 969 - 976
