4-甲氧基-2-苯基苯乙酮合成路线 （共 128 条）
反应条件
1: S2O8(2-), Fe(ClO4), HClO4 / Cu(ClO4)2 / acetonitrile; H2O / Ambient temperature 2: NaOH / tetrahydrofuran; H2O 3: S2O8(2-), HClO4 / Cu(ClO4)2 / acetonitrile; H2O / 0.42 h / 83 °C / other reaction conditions, other substrate 4: pyridine-chlorochromate View Scheme
参考文献
Journal of Organic Chemistry, , vol. 49, # 9 p. 1607 - 1613
反应条件
hydrogenchloride; sodium hydroxide; zinc diiodide; trifluoroacetic acid; lithium diisopropyl amide in tetrahydrofuran; n-heptane; dichloromethane; water
反应条件
bis-triphenylphosphine-palladium(II) chloride; triethylamine in tetrahydrofuran T=80°C; 3 h; Schlenk tubeInert atmosphere;
参考文献
Rao, Maddali L.N.; Giri, Somnath; Jadhav, Deepak N.
Tetrahedron Letters, 2009 , vol. 50, # 45 p. 6133 - 6138
反应条件
water; palladium diacetate; potassium hydrogencarbonate; tri-cyclo-hexyl-phosphine T=100°C; Suzuki coupling; P=7500.75 Torr; 20 h; Inert atmosphere;
参考文献
Wu, Xiao-Feng; Neumann, Helfried; Beller, Matthias
Advanced Synthesis and Catalysis, 2011 , vol. 353, # 5 p. 788 - 792
反应条件
Ni(PCy3)2Cl2; sodium t-butanolate in N,N-dimethyl-formamide; toluene T=100°C; Suzuki-Miyaura coupling; 0.666667 h; Inert atmosphere;
参考文献
Huang, Kun; Li, Gang; Huang, Wei-Ping; Yu, Da-Gang; Shi, Zhang-Jie
Chemical Communications, 2011 , vol. 47, # 25 p. 7224 - 7226
反应条件
tris-(dibenzylideneacetone)dipalladium(0); bis[2-(diphenylphosphino)phenyl] ether; sodium t-butanolate in tetrahydrofuran T=70°C; 3 h; Schlenk techniqueInert atmosphere;
参考文献
Mehta, Vaibhav P.; Garcia-Lopez, Jose-Antonio; Greaney, Michael F.
Angewandte Chemie - International Edition, 2014 , vol. 53, # 6 p. 1529 - 1533
Angew. Chem., 2014 , vol. 126, # 6 p. 1555 - 1559,5
反应条件
NiBr2bipy; tetra-n-butylammonium tetrafluoroborate in N,N-dimethyl-formamide Electrochemical reaction;
参考文献
Dolhem, Eric; Barhdadi, Rachid; Folest, Jean Claude; Nedelec, Jean Yves; Troupel, Michel
Tetrahedron, 2001 , vol. 57, # 3 p. 525 - 529
反应条件
caesium carbonate in tetrahydrofuran; tert-butyl methyl ether 34 h; Product distribution / selectivity;
参考文献
US2007/149564 A1, ;
Page/Page column 58 ;
反应条件
potassium cyanide in N,N-dimethyl-formamide 1 h; Heating;
参考文献
Heterocycles, , vol. 45, # 1 p. 1 - 5
反应条件
1: NaOH / tetrahydrofuran; H2O 2: S2O8(2-), HClO4 / Cu(ClO4)2 / acetonitrile; H2O / 0.42 h / 83 °C / other reaction conditions, other substrate 3: pyridine-chlorochromate View Scheme
参考文献
Journal of Organic Chemistry, , vol. 49, # 9 p. 1607 - 1613
