4-甲氧基-2-苯基苯乙酮合成路线 （共 128 条）
反应条件
zinc oxide T=20°C; Friedel-Crafts acylation; 0.0833333 h;
参考文献
Sarvari, Mona Hosseini; Sharghi, Hashem
Journal of Organic Chemistry, 2004 , vol. 69, # 20 p. 6953 - 6956
反应条件
ammonium chloride; bipyridine-cyclopalladated ferrocenylimine complex in water T=100°C; 24 h;
参考文献
Yu, Ajuan; Li, Jingya; Cui, Mengjun; Wu, Yangjie
Synlett, 2007 , # 19 p. 3063 - 3067
反应条件
scandium tris(trifluoromethanesulfonate) in toluene T=-78°C; 0.166667 h; Inert atmosphere;
参考文献
Wommack, Andrew J.; Moebius, David C.; Travis, Austin L.; Kingsbury, Jason S.
Organic Letters, 2009 , vol. 11, # 15 p. 3202 - 3205
反应条件
hydrogenchloride; AlCl3; Nalco silica sol 1060 in dichloromethane; methoxybenzene
参考文献
The Upjohn Company
Patent: US5098918 A1, 1992 ;
反应条件
pyrrolidine; 1,3-bis-(diphenylphosphino)propane; bis(dibenzylideneacetone)-palladium(0) in N,N-dimethyl-formamide T=115°C; Heck reaction; 6 h; Molecular sieve;
参考文献
Ruan, Jiwu; Saidi, Ourida; Iggo, Jonathan A.; Xiao, Jianliang
Journal of the American Chemical Society, 2008 , vol. 130, # 32 p. 10510 - 10511
反应条件
palladium diacetate; 1,4-di(diphenylphosphino)-butane; zinc in 1,4-dioxane T=100°C; Negishi coupling reaction; P=7500.75 Torr; 16 h; Inert atmosphereAutoclave;
参考文献
Wu, Xiao-Feng; Schranck, Johannes; Neumann, Helfried; Beller, Matthias
Chemistry - An Asian Journal, 2012 , vol. 7, # 1 p. 40 - 44
反应条件
toluene-4-sulfonic acid in ethanol T=120°C; 0.5 h; microwave irradiation;
参考文献
Le Bras, Gaelle; Provot, Olivier; Peyrat, Jean-Francois; Alami, Mouad; Brion, Jean-Daniel
Tetrahedron Letters, 2006 , vol. 47, # 31 p. 5497 - 5501
反应条件
1: With sodium hydrogencarbonate; bis(η3-allyl-μ-chloropalladium(II)); Tedicyp in N,N-dimethyl-formamide T=150°C; Heck reaction; 20 h; 2: With hydrogenchloride in tetrahydrofuran T=25°C; Further stages.;
参考文献
Battace, Ahmed; Feuerstein, Marie; Lemhadri, Mhamed; Zair, Touriya; Doucet, Henri; Santelli, Maurice
European Journal of Organic Chemistry, 2007 , # 19 p. 3122 - 3132
反应条件
palladium diacetate; 1,4-di(diphenylphosphino)-butane in tetrahydrofuran T=90°C; P=1500.15 Torr; 1 h; Sealed tubeMicrowave irradiation; chemoselective reaction;
参考文献
Motwani, Hitesh V.; Larhed, Mats
European Journal of Organic Chemistry, 2013 , # 22 p. 4729 - 4733
反应条件
trans-di(μ-acetato)bis[o-(di-o-tolylphosphino)benzyl]dipalladium(II); 1,8-diazabicyclo[5.4.0]undec-7-ene; [(t-Bu)3PH]BF4 in tetrahydrofuran T=120°C; P=2250.23 Torr; 0.5 h; Microwave irradiationSealed tube; chemoselective reaction;
参考文献
Motwani, Hitesh V.; Larhed, Mats
European Journal of Organic Chemistry, 2013 , # 22 p. 4729 - 4733
