1,1,3,3-四甲氧基丙烷合成路线 （共 127 条）
反应条件
tetraphosphorus decasulfide; sulfur in pyridine T=130°C; 0.5 h;
参考文献
Charbonnel-Jobic, Gaelle; Guemas, Jean-Pierre; Adelaere, Bruno; Parrain, Jean-Luc; Quintard, Jean-Paul
Bulletin de la Societe Chimique de France, 1995 , vol. 132, p. 624 - 636
反应条件
titanium tetrachloride in dichloromethane T=-78 - 20°C; 20 h;
参考文献
Reim, Stefanie; Langer, Peter
Tetrahedron Letters, 2008 , vol. 49, # 14 p. 2329 - 2332
反应条件
1: With trimethylsilyl trifluoromethanesulfonate in dichloromethane T=-78 - 20°C; 2: With hydrogenchloride in dichloromethane Further stages.;
参考文献
Sher, Muhammad; Tam Dang; Ahmed, Zafar; Rashid, Muhammad A.; Fischer, Christine; Langer, Peter
Journal of Organic Chemistry, 2007 , vol. 72, # 16 p. 6284 - 6286
反应条件
hydrogenchloride in water; isopropyl alcohol T=0 - 60°C; 6 h;
参考文献
Perez-Balado, Carlos; Willemsens, Albert; Ormerod, Dominic; Aelterman, Wim; Mertens, Narda
Organic Process Research and Development, 2007 , vol. 11, # 2 p. 237 - 240
反应条件
1: 4-amino-2-methoxy-benzoic acid methyl ester With hydrogenchloride; sodium nitrite in water T=0°C; 0.333333 h; 2: With tin(ll) chloride in water T=0°C; 1.5 h; 3: malonaldehyde bis(dimethyl acetal); ethanol in ethanol Heating / reflux;
参考文献
SB PHARMCO PUERTO RICO INC; NEUROCRINE BIOSCIENCES INC
Patent: WO2005/63756 A1, 2005 ;
Location in patent: Page/Page column 19 ;
WO 2005/063756 A1
参考文献
Gen. Aniline and Film Corp.
Patent: DE822086 , 1951 ;
DRP/DRBP Org.Chem.
反应条件
hydrogenchloride; water in ethanol T=0 - 20°C; 1.25 h;
参考文献
Brun, Matthias A.; Tan, Kui-Thong; Nakata, Eiji; Hinner, Marlon J.; Johnsson, Kai
Journal of the American Chemical Society, 2009 , vol. 131, p. 5873 - 5884
反应条件
hydrogenchloride in water T=50°C; 3 h;
参考文献
CENTRE NATIONAL DE LA RECHERCHE SCIENTIFIQUE (CNRS); PIERRE FABRE MEDICAMENT; Guminski, Yves; Imbert, Thierry; Pesnel, Sabrina; Pillon, Arnaud; Le Pape, Alain; Lerondel, Stephanie
Patent: US2013/183247 A1, 2013 ;
Location in patent: Paragraph 0133; 0134 ;
反应条件
phosphoric acid T=20°C; 40 h;
参考文献
Bi, Lanrong; Zhang, Yue; Zhao, Ming; Wang, Chao; Chan, Priscilla; Tok, Jeffrey B.-H.; Peng, Shiqi
Bioorganic and Medicinal Chemistry, 2005 , vol. 13, # 19 p. 5640 - 5646
反应条件
zinc(II) chloride in hydrogenchloride; ethanol 1 h; Heating;
参考文献
Lynch; Khan; Teo; Pedrotti
Canadian Journal of Chemistry, 1988 , vol. 66, # 3 p. 420-428
