ethoxylated alkylphenols mixt. in cyclohexane; water mixing AgNO3 and NaH2PO2 microemulsions at room temp.; detd. by x-ray scattering and electron spectroscopy;
ethoxylated alkylphenols mixt. in cyclohexane; water mixing AgNO3 and NaH2PO2 microemulsions at room temp.; detd. by x-ray scattering and electron spectroscopy;
in neat (no solvent) addn. of anhydrous H2SO4 to dry NaH2PO2; shaking the solidified soln. after with abs. alcohol after 2 days;; filtration of Na2SO4; evapn. of alcohol at ambient pressure, then in vacuum; Crystn. on cooling with a freezing mixture;;
in water-d2
treatment of NaH2PO2*H2O with DCl in D2O under Ar, stirring for 1 h, removal of solvent in vacuo, adding D2O and DCl, stirring for addnl. 30 min; not isolated;
参考文献
Yorimitsu; Shinokubo; Oshima
Bulletin of the Chemical Society of Japan, 2001 , vol. 74, # 2 p. 225 - 235
